1-(4-(cyclopenta-2,4-dienyldimethylsilyl)phenyl)-N,N-diethylmethanamine

Base Information

Chemical Name:1-(4-(cyclopenta-2,4-dienyldimethylsilyl)phenyl)-N,N-diethylmethanamine
CAS No.:1384460-90-5
Molecular Formula:C₁₈H₂₇NSi
Molecular Weight:285.505
Hs Code.:

Synonyms:1-(4-(cyclopenta-2,4-dienyldimethylsilyl)phenyl)-N,N-diethylmethanamine

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 1-(4-(cyclopenta-2,4-dienyldimethylsilyl)phenyl)-N,N-diethylmethanamine

Chemical Property:

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Technology Process of 1-(4-(cyclopenta-2,4-dienyldimethylsilyl)phenyl)-N,N-diethylmethanamine

There total 1 articles about 1-(4-(cyclopenta-2,4-dienyldimethylsilyl)phenyl)-N,N-diethylmethanamine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 4885-19-2
1-(4-bromophenyl)-N,N-diethylmethanamine

: 1384460-90-5
1-(4-(cyclopenta-2,4-dienyldimethylsilyl)phenyl)-N,N-diethylmethanamine

Guidance literature:: Multi-step reaction with 2 steps

1.1: magnesium / tetrahydrofuran / 0 °C

1.2: 0 - 20 °C

2.1: n-butyllithium / tetrahydrofuran; hexane / 16 h

With n-butyllithium; magnesium; In tetrahydrofuran; hexane;
DOI:10.1021/om300227h

Reference yield: 60.0%

: 1384460-90-5
1-(4-(cyclopenta-2,4-dienyldimethylsilyl)phenyl)-N,N-diethylmethanamine

: 7550-45-0
titanium tetrachloride

: 1384264-09-8
bis-[((4-N,N-diethylmethanamine)dimethylsilane)-cyclopentadienyl]titanium(IV) dichloride

Guidance literature:: 1-(4-(cyclopenta-2,4-dienyldimethylsilyl)phenyl)-N,N-diethylmethanamine; With n-butyllithium; In tetrahydrofuran; hexane; at -78 ℃; for 0.5h;

titanium tetrachloride; In tetrahydrofuran; hexane; toluene; at 20 ℃;
DOI:10.1021/om300227h