HOC₆H₄(CH₂)2GeCl₃

Base Information

• Chemical Name: HOC₆H₄(CH₂)2GeCl₃
• CAS No.: 232946-67-7
• Molecular Formula: C₈H₉Cl₃GeO
• Molecular Weight: 300.108

Synonyms:HOC₆H₄(CH₂)2GeCl₃

Chemical Property of HOC₆H₄(CH₂)2GeCl₃

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Technology Process of HOC₆H₄(CH₂)2GeCl₃

There total 1 articles about HOC₆H₄(CH₂)2GeCl₃ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 91.0%

germanium(II) chloride-dioxane complex + 4-(2-chloroethyl)phenol (28145-35-9) → HOC6H4(CH2)2GeCl3 (232946-67-7)

Guidance literature:

In 1,4-dioxane; High Pressure; heating at 140°C for 16 h;

DOI:10.1039/a900915i

Reference yield: 82.0%

HOC6H4(CH2)2GeCl3 (232946-67-7) + methylmagnesium bromide (75-16-1) → 4-(2-(trimethylgermyl)ethyl)phenol (232946-68-8)

Guidance literature:

In toluene; refluxing for 16 h;

DOI:10.1039/a900915i

upstream raw materials:

4-(2-chloroethyl)phenol

Downstream raw materials:

4-(2-(trimethylgermyl)ethyl)phenol

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