4-(4-Heptyl-phenyl)-N¹-[1-phenyl-meth-(Z)-ylidene]-imidazole-1,2-diamine

Base Information

• Chemical Name: 4-(4-Heptyl-phenyl)-N¹-[1-phenyl-meth-(Z)-ylidene]-imidazole-1,2-diamine
• CAS No.: 81539-67-5
• Molecular Formula: C₂₃H₂₈N₄
• Molecular Weight: 360.502
• Mol file: 81539-67-5.mol

Synonyms:4-(4-Heptyl-phenyl)-N¹-[1-phenyl-meth-(Z)-ylidene]-imidazole-1,2-diamine

Chemical Property of 4-(4-Heptyl-phenyl)-N¹-[1-phenyl-meth-(Z)-ylidene]-imidazole-1,2-diamine

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of 4-(4-Heptyl-phenyl)-N¹-[1-phenyl-meth-(Z)-ylidene]-imidazole-1,2-diamine

There total 3 articles about 4-(4-Heptyl-phenyl)-N¹-[1-phenyl-meth-(Z)-ylidene]-imidazole-1,2-diamine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 54.0%

2-Chloro-1-(4-heptyl-phenyl)-ethanone (81539-58-4) + 2-benzylidenehydrazinecarboximidamide (3357-37-7) → 4-(4-Heptyl-phenyl)-N1-[1-phenyl-meth-(Z)-ylidene]-imidazole-1,2-diamine (81539-67-5)

Guidance literature:

In ethanol; for 3h; Heating;

DOI:10.1007/BF00512966

Reference yield:

4'-heptylacetophenone (37593-03-6) → 4-(4-Heptyl-phenyl)-N1-[1-phenyl-meth-(Z)-ylidene]-imidazole-1,2-diamine (81539-67-5)

Guidance literature:

Multi-step reaction with 2 steps

1: Br₂ / acetic acid / 40 °C

2: ethanol / 2 h / Heating

With bromine; In ethanol; acetic acid;

DOI:10.1007/BF00512966

Reference yield:

ω-Brom-p-(n-heptyl)acetophenon (64328-70-7) + 2-benzylidenehydrazinecarboximidamide (3357-37-7) → 4-(4-Heptyl-phenyl)-N1-[1-phenyl-meth-(Z)-ylidene]-imidazole-1,2-diamine (81539-67-5) + C46H52N8 (81539-62-0)

Guidance literature:

In ethanol; for 2h; Yield given; Heating;

DOI:10.1007/BF00512966

upstream raw materials:

ω-Brom-p-(n-heptyl)acetophenon

2-benzylidenehydrazinecarboximidamide

2-Chloro-1-(4-heptyl-phenyl)-ethanone

4'-heptylacetophenone

Downstream raw materials:

4-(4-Heptyl-phenyl)-imidazole-1,2-diamine