Technology Process of C17H18F2N2O3S
There total 3 articles about C17H18F2N2O3S which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
With
dicyclohexyl-(2',6'-dimethoxybiphenyl-2-yl)-phosphane; tris-(dibenzylideneacetone)dipalladium(0); caesium carbonate;
In
1,4-dioxane;
at 120 ℃;
for 0.666667h;
Microwave irradiation;
Inert atmosphere;
- Guidance literature:
-
Multi-step reaction with 3 steps
1: ethyl acetate / 3 h / 25 °C
2: N-ethyl-N,N-diisopropylamine; HATU / dichloromethane / 2 h / 20 °C
3: dicyclohexyl-(2',6'-dimethoxybiphenyl-2-yl)-phosphane; tris-(dibenzylideneacetone)dipalladium(0); caesium carbonate / 1,4-dioxane / 0.67 h / 120 °C / Microwave irradiation; Inert atmosphere
With
dicyclohexyl-(2',6'-dimethoxybiphenyl-2-yl)-phosphane; tris-(dibenzylideneacetone)dipalladium(0); caesium carbonate; N-ethyl-N,N-diisopropylamine; HATU;
In
1,4-dioxane; dichloromethane; ethyl acetate;
- Guidance literature:
-
Multi-step reaction with 2 steps
1: N-ethyl-N,N-diisopropylamine; HATU / dichloromethane / 2 h / 20 °C
2: dicyclohexyl-(2',6'-dimethoxybiphenyl-2-yl)-phosphane; tris-(dibenzylideneacetone)dipalladium(0); caesium carbonate / 1,4-dioxane / 0.67 h / 120 °C / Microwave irradiation; Inert atmosphere
With
dicyclohexyl-(2',6'-dimethoxybiphenyl-2-yl)-phosphane; tris-(dibenzylideneacetone)dipalladium(0); caesium carbonate; N-ethyl-N,N-diisopropylamine; HATU;
In
1,4-dioxane; dichloromethane;