8-isopropyl-4,4,12-triphenyl-2,3,11-trioxa-8-azatricyclo[4.4.3.0(1,6)]tridec-12-en-7-one

Base Information

• Chemical Name: 8-isopropyl-4,4,12-triphenyl-2,3,11-trioxa-8-azatricyclo[4.4.3.0(1,6)]tridec-12-en-7-one
• CAS No.: 913835-03-7
• Molecular Formula: C₃₀H₂₉NO₄
• Molecular Weight: 467.565

Synonyms:8-isopropyl-4,4,12-triphenyl-2,3,11-trioxa-8-azatricyclo[4.4.3.0(1,6)]tridec-12-en-7-one

Chemical Property of 8-isopropyl-4,4,12-triphenyl-2,3,11-trioxa-8-azatricyclo[4.4.3.0(1,6)]tridec-12-en-7-one

Chemical Property:

Purity/Quality:

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• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of 8-isopropyl-4,4,12-triphenyl-2,3,11-trioxa-8-azatricyclo[4.4.3.0(1,6)]tridec-12-en-7-one

There total 4 articles about 8-isopropyl-4,4,12-triphenyl-2,3,11-trioxa-8-azatricyclo[4.4.3.0(1,6)]tridec-12-en-7-one which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 86.0%

1-isopropyl-3-(2-oxo-2-phenylethyl)piperidine-2,4-dione (913834-62-5) + 1,1-Diphenylethylene (530-48-3) → 3-isopropyl-8,11,11-triphenyl-7,12-dioxa-3-aza-tricyclo[4.3.3.01,6]dodec-8-en-2-one + 8-isopropyl-4,4,12-triphenyl-2,3,11-trioxa-8-azatricyclo[4.4.3.0(1,6)]tridec-12-en-7-one (913835-03-7)

Guidance literature:

With manganese triacetate; In acetic acid; for 0.166667h; Heating;

DOI:10.1016/j.tetlet.2006.07.090

Reference yield: 67.0%

1-isopropyl-3-(2-oxo-2-phenylethyl)piperidine-2,4-dione (913834-62-5) + 1,1-Diphenylethylene (530-48-3) → 8-isopropyl-4,4,12-triphenyl-2,3,11-trioxa-8-azatricyclo[4.4.3.0(1,6)]tridec-12-en-7-one (913835-03-7)

Guidance literature:

With air; manganese triacetate; In acetic acid; at 20 - 100 ℃; for 7.5h;

DOI:10.1515/HC.2008.14.1-2.21

Reference yield: 51.0%

1-isopropyl-3-(2-oxo-2-phenylethyl)piperidine-2,4-dione (913834-62-5) + 1,1-Diphenylethylene (530-48-3) + manganese triacetate (638-38-0,993-02-2,2180-18-9,15411-95-7,22981-23-3,27004-39-3) → 3-isopropyl-8,11,11-triphenyl-7,12-dioxa-3-aza-tricyclo[4.3.3.01,6]dodec-8-en-2-one + 8-isopropyl-4,4,12-triphenyl-2,3,11-trioxa-8-azatricyclo[4.4.3.0(1,6)]tridec-12-en-7-one (913835-03-7) + acetic acid 5-isopropyl-4-oxo-3a-(2-oxo-2-phenyl-ethyl)-2,2-diphenyl-hexahydro-furo[3,2-c]pyridin-7a-yl ester + acetic acid 2-[1-isopropyl-2,4-dioxo-3-(2-oxo-2-phenyl-ethyl)-piperidin-3-yl]-1,1-diphenyl-ethyl ester

Guidance literature:

In acetic acid; for 0.0166667h; Heating;

DOI:10.1016/j.tetlet.2006.07.090

upstream raw materials:

1-isopropyl-3-(2-oxo-2-phenylethyl)piperidine-2,4-dione

1,1-Diphenylethylene

manganese triacetate

Downstream raw materials:

1-isopropyl-3,3-bis(2-oxo-2-phenylethyl)piperidine-2,4-dione

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