C₃₇H₅₀N₂O₄

Base Information

Chemical Name:C₃₇H₅₀N₂O₄
CAS No.:1055981-27-5
Molecular Formula:C₃₇H₅₀N₂O₄
Molecular Weight:586.815
Hs Code.:

C<sub>37</sub>H<sub>50</sub>N<sub>2</sub>O<sub>4</sub>

Synonyms:C₃₇H₅₀N₂O₄

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Chemical Property of C₃₇H₅₀N₂O₄

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Technology Process of C₃₇H₅₀N₂O₄

There total 14 articles about C₃₇H₅₀N₂O₄ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 99.0%

: 1055981-25-3
C₃₆H₄₈N₂O₄

: 74-88-4
methyl iodide

: 1055981-27-5
C₃₇H₅₀N₂O₄

Guidance literature:: With potassium hexamethyldisilazane; In tetrahydrofuran; toluene; at -78 - 20 ℃; for 18.5h; Inert atmosphere;
DOI:10.1021/jm900305z

Reference yield:

: 878204-96-7
IPI-269609

: 1055981-27-5
C₃₇H₅₀N₂O₄

Guidance literature:: Multi-step reaction with 9 steps

1.1: hydrogen / palladium 10% on activated carbon / pyridine / 20 °C / 760.05 Torr

2.1: triethylamine / tetrahydrofuran / 1 h / 20 °C

3.1: potassium tert-butylate / tert-butyl alcohol / 0.25 h / 20 °C

3.2: 48 h / 20 °C

4.1: 2,3-dicyano-5,6-dichloro-p-benzoquinone / toluene / 0.5 h / 20 °C

5.1: Wilkinson's catalyst / toluene / 0.5 h / 80 °C

6.1: hydroxylamine hydrochloride; sodium acetate / ethanol; water / 0.5 h / 20 °C

7.1: pyridine / 0.5 h / 20 °C

8.1: hydrogenchloride / methanol; water / 17 h / 60 °C

9.1: potassium hexamethylsilazane / tetrahydrofuran; toluene / 0.5 h / -78 °C

9.2: -78 - 25 °C

With pyridine; hydrogenchloride; hydroxylamine hydrochloride; potassium tert-butylate; hydrogen; sodium acetate; potassium hexamethylsilazane; triethylamine; 2,3-dicyano-5,6-dichloro-p-benzoquinone; Wilkinson's catalyst; palladium 10% on activated carbon; In tetrahydrofuran; pyridine; methanol; ethanol; water; toluene; tert-butyl alcohol;

Reference yield:

: 1037210-47-1
C₃₆H₄₉NO₄

: 1055981-27-5
C₃₇H₅₀N₂O₄

Guidance literature:: Multi-step reaction with 7 steps

1.1: potassium tert-butylate / tert-butyl alcohol / 0.25 h / 20 °C

1.2: 48 h / 20 °C

2.1: 2,3-dicyano-5,6-dichloro-p-benzoquinone / toluene / 0.5 h / 20 °C

3.1: Wilkinson's catalyst / toluene / 0.5 h / 80 °C

4.1: hydroxylamine hydrochloride; sodium acetate / ethanol; water / 0.5 h / 20 °C

5.1: pyridine / 0.5 h / 20 °C

6.1: hydrogenchloride / methanol; water / 17 h / 60 °C

7.1: potassium hexamethylsilazane / tetrahydrofuran; toluene / 0.5 h / -78 °C

7.2: -78 - 25 °C

With pyridine; hydrogenchloride; hydroxylamine hydrochloride; potassium tert-butylate; sodium acetate; potassium hexamethylsilazane; 2,3-dicyano-5,6-dichloro-p-benzoquinone; Wilkinson's catalyst; In tetrahydrofuran; methanol; ethanol; water; toluene; tert-butyl alcohol;