C₂₃H₂₂Br₂O₂

Base Information

Chemical Name:C₂₃H₂₂Br₂O₂
CAS No.:1419387-69-1
Molecular Formula:C₂₃H₂₂Br₂O₂
Molecular Weight:490.234
Hs Code.:

C<sub>23</sub>H<sub>22</sub>Br<sub>2</sub>O<sub>2</sub>

Synonyms:C₂₃H₂₂Br₂O₂

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Chemical Property of C₂₃H₂₂Br₂O₂

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Technology Process of C₂₃H₂₂Br₂O₂

There total 8 articles about C₂₃H₂₂Br₂O₂ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 88.0%

: 1419387-66-8
C₂₃H₂₄O₂

: 1419387-69-1
C₂₃H₂₂Br₂O₂

Guidance literature:: C₂₃H₂₄O₂; With t-butyldimethylsiyl triflate; N-ethyl-N,N-diisopropylamine; In dichloromethane; at 20 ℃; for 2h;

With N-Bromosuccinimide; In tetrahydrofuran; at 0 ℃; for 4h;

Reference yield:

: 13336-31-7
4-methoxylindanone

: 1419387-69-1
C₂₃H₂₂Br₂O₂

Guidance literature:: Multi-step reaction with 7 steps

1.1: potassium tert-butylate / toluene / 3.5 h / 80 °C / Inert atmosphere; Cooling with ice

2.1: triethylsilane; trifluoroacetic acid / 40 °C / Cooling with ice

3.1: aluminum (III) chloride / 1,2-dichloro-ethane / 2 h / 20 °C

4.1: boron tribromide / dichloromethane / 24 h / -40 - 20 °C

5.1: pyridine / dichloromethane / 2 h / 0 - 20 °C

6.1: tetrakis(triphenylphosphine) palladium⁽⁰⁾; potassium carbonate / 1,2-dimethoxyethane; water / 5 h / 90 °C

7.1: t-butyldimethylsiyl triflate; N-ethyl-N,N-diisopropylamine / dichloromethane / 2 h / 20 °C / Cooling with ice

7.2: 4 h / 0 °C

With pyridine; triethylsilane; aluminum (III) chloride; tetrakis(triphenylphosphine) palladium⁽⁰⁾; t-butyldimethylsiyl triflate; potassium tert-butylate; boron tribromide; potassium carbonate; N-ethyl-N,N-diisopropylamine; trifluoroacetic acid; In 1,2-dimethoxyethane; dichloromethane; water; 1,2-dichloro-ethane; toluene;

Reference yield:

: 1419386-97-2
C₁₄H₁₈O

: 1419387-69-1
C₂₃H₂₂Br₂O₂

Guidance literature:: Multi-step reaction with 5 steps

1.1: aluminum (III) chloride / 1,2-dichloro-ethane / 2 h / 20 °C

2.1: boron tribromide / dichloromethane / 24 h / -40 - 20 °C

3.1: pyridine / dichloromethane / 2 h / 0 - 20 °C

4.1: tetrakis(triphenylphosphine) palladium⁽⁰⁾; potassium carbonate / 1,2-dimethoxyethane; water / 5 h / 90 °C

5.1: t-butyldimethylsiyl triflate; N-ethyl-N,N-diisopropylamine / dichloromethane / 2 h / 20 °C / Cooling with ice

5.2: 4 h / 0 °C

With pyridine; aluminum (III) chloride; tetrakis(triphenylphosphine) palladium⁽⁰⁾; t-butyldimethylsiyl triflate; boron tribromide; potassium carbonate; N-ethyl-N,N-diisopropylamine; In 1,2-dimethoxyethane; dichloromethane; water; 1,2-dichloro-ethane;