ethyl 2-(3-amino-3-{3-[(E)-2-(7-chloroquinolin-2-yl)vinyl]phenyl}propyl)benzoate

Base Information

Chemical Name:ethyl 2-(3-amino-3-{3-[(E)-2-(7-chloroquinolin-2-yl)vinyl]phenyl}propyl)benzoate
CAS No.:1429878-92-1
Molecular Formula:C₂₉H₂₇ClN₂O₂
Molecular Weight:470.999
Hs Code.:

Synonyms:ethyl 2-(3-amino-3-{3-[(E)-2-(7-chloroquinolin-2-yl)vinyl]phenyl}propyl)benzoate

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Chemical Property of ethyl 2-(3-amino-3-{3-[(E)-2-(7-chloroquinolin-2-yl)vinyl]phenyl}propyl)benzoate

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Technology Process of ethyl 2-(3-amino-3-{3-[(E)-2-(7-chloroquinolin-2-yl)vinyl]phenyl}propyl)benzoate

There total 4 articles about ethyl 2-(3-amino-3-{3-[(E)-2-(7-chloroquinolin-2-yl)vinyl]phenyl}propyl)benzoate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 94.0%

: 64-17-5
ethanol

: 1429878-89-6
2-(3-amino-3-{3-[(E)-2-(7-chloroquinolin-2-yl)vinyl]phenyl}propyl)benzoic acid

: 1429878-92-1
ethyl 2-(3-amino-3-{3-[(E)-2-(7-chloroquinolin-2-yl)vinyl]phenyl}propyl)benzoate

Guidance literature:: With sulfuric acid; for 3h; Reflux;

Reference yield:

: 149968-11-6
methyl 2-(3-(3-(2-(7-chloro-2-quinolinyl)ethenyl)phenyl)-3-oxopropyl)benzoate

: 1429878-92-1
ethyl 2-(3-amino-3-{3-[(E)-2-(7-chloroquinolin-2-yl)vinyl]phenyl}propyl)benzoate

Guidance literature:: Multi-step reaction with 4 steps

1: sodium tetrahydroborate; methanol / dichloromethane / 1 h / Inert atmosphere

2: acetic acid; sulfuric acid / water / 24 h / 0 - 20 °C

3: hydrogenchloride; water / 1,4-dioxane / 110 °C

4: sulfuric acid / dichloromethane

With hydrogenchloride; methanol; sodium tetrahydroborate; sulfuric acid; water; acetic acid; In 1,4-dioxane; dichloromethane; water;

Reference yield:

: methyl 2-(3-(3-(2-(7-chloro-2-quinolinyl)-ethenyl)phenyl)-3(R)-3-hydroxypropyl)benzoate

: 1429878-92-1
ethyl 2-(3-amino-3-{3-[(E)-2-(7-chloroquinolin-2-yl)vinyl]phenyl}propyl)benzoate

Guidance literature:: Multi-step reaction with 3 steps

1: acetic acid; sulfuric acid / water / 24 h / 0 - 20 °C

2: hydrogenchloride; water / 1,4-dioxane / 110 °C

3: sulfuric acid / dichloromethane

With hydrogenchloride; sulfuric acid; water; acetic acid; In 1,4-dioxane; dichloromethane; water;