(Z)-2-(1-(4-methoxyphenyl)-2-phenylvinyl)-4,4,5,5-tetramethyl-1,3,2-dioxaborolane

Base Information

Chemical Name:(Z)-2-(1-(4-methoxyphenyl)-2-phenylvinyl)-4,4,5,5-tetramethyl-1,3,2-dioxaborolane
CAS No.:1351458-48-4
Molecular Formula:C₂₁H₂₅BO₃
Molecular Weight:336.239
Hs Code.:

Synonyms:(Z)-2-(1-(4-methoxyphenyl)-2-phenylvinyl)-4,4,5,5-tetramethyl-1,3,2-dioxaborolane

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of (Z)-2-(1-(4-methoxyphenyl)-2-phenylvinyl)-4,4,5,5-tetramethyl-1,3,2-dioxaborolane

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Technology Process of (Z)-2-(1-(4-methoxyphenyl)-2-phenylvinyl)-4,4,5,5-tetramethyl-1,3,2-dioxaborolane

There total 5 articles about (Z)-2-(1-(4-methoxyphenyl)-2-phenylvinyl)-4,4,5,5-tetramethyl-1,3,2-dioxaborolane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 88.0%

: 1351458-41-7
(Z)-2-(1-iodo-2-phenylvinyl)-4,4,5,5-tetramethyl-1,3,2-dioxaborolane

: 82303-13-7
(4-methoxyphenyl)zinc(II) bromide

: 1351458-48-4
(Z)-2-(1-(4-methoxyphenyl)-2-phenylvinyl)-4,4,5,5-tetramethyl-1,3,2-dioxaborolane

Guidance literature:: With bis(tri-t-butylphosphine)palladium⁽⁰⁾; In tetrahydrofuran; at 23 ℃; Inert atmosphere;
DOI:10.1002/adsc.201100420

Reference yield:

: C₁₅H₁₃O₂^(1-)*Li⁽¹⁺⁾

: 73183-34-3
bis(pinacol)diborane

: 1351458-48-4
(Z)-2-(1-(4-methoxyphenyl)-2-phenylvinyl)-4,4,5,5-tetramethyl-1,3,2-dioxaborolane

Guidance literature:: With magnesium methanolate; In toluene; at 130 ℃; for 12h; stereoselective reaction; Inert atmosphere;
DOI:10.1002/anie.201909235

Reference yield:

: 7380-78-1
4-(phenylethynyl)anisole

: 25015-63-8
4,4,5,5-tetramethyl-[1,3,2]-dioxaboralane

: 1351458-48-4
(Z)-2-(1-(4-methoxyphenyl)-2-phenylvinyl)-4,4,5,5-tetramethyl-1,3,2-dioxaborolane

: (Z)-2-[2-(4-methoxyphenyl)-1-phenylvinyl]-4,4,5,5-tetramethyl-1,3,2-dioxaborolane

Guidance literature:: 4,4,5,5-tetramethyl-[1,3,2]-dioxaboralane; With 4,5-bis(diphenylphosphino)-9,9-dimethylxanthene; cobalt acetylacetonate; In tetrahydrofuran; at 20 ℃; for 0.25h; Inert atmosphere; Schlenk technique;

4-(phenylethynyl)anisole; In tetrahydrofuran; at 20 ℃; for 16h; Overall yield = 95 percent; Overall yield = 128.17 mg; Inert atmosphere; Schlenk technique;
DOI:10.1021/acs.orglett.1c02854