1-(1,2-μ,η2-(O,O')-carboxylato-(1,2-μ-hydrido)-1,1,1,1,2,2,2,3,3,3-decacarbonyl-triangulo-triosmium)-2-acetylferrocene

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Chemical Name:1-(1,2-μ,η2-(O,O')-carboxylato-(1,2-μ-hydrido)-1,1,1,1,2,2,2,3,3,3-decacarbonyl-triangulo-triosmium)-2-acetylferrocene
CAS No.:458556-22-4
Molecular Formula:C₂₃H₁₂FeO₁₃Os₃
Molecular Weight:1122.79
Hs Code.:

Synonyms:1-(1,2-μ,η2-(O,O')-carboxylato-(1,2-μ-hydrido)-1,1,1,1,2,2,2,3,3,3-decacarbonyl-triangulo-triosmium)-2-acetylferrocene

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Chemical Property of 1-(1,2-μ,η2-(O,O')-carboxylato-(1,2-μ-hydrido)-1,1,1,1,2,2,2,3,3,3-decacarbonyl-triangulo-triosmium)-2-acetylferrocene

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Technology Process of 1-(1,2-μ,η2-(O,O')-carboxylato-(1,2-μ-hydrido)-1,1,1,1,2,2,2,3,3,3-decacarbonyl-triangulo-triosmium)-2-acetylferrocene

There total 1 articles about 1-(1,2-μ,η2-(O,O')-carboxylato-(1,2-μ-hydrido)-1,1,1,1,2,2,2,3,3,3-decacarbonyl-triangulo-triosmium)-2-acetylferrocene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 9.7%

: 174742-53-1
(μ-H)Os3(μ-O2CC5H4FeCp)(CO)10

: 75-36-5
acetyl chloride

: 1271-42-7
ferrocenecarboxylic acid

: (μ-H)Os3(μ-Cl)(CO)10

: 458556-22-4
1-(1,2-μ,η2-(O,O')-carboxylato-(1,2-μ-hydrido)-1,1,1,1,2,2,2,3,3,3-decacarbonyl-triangulo-triosmium)-2-acetylferrocene

: 458556-20-2
1-(1,2-μ,η2-(O,O')-carboxylato-(1,2-μ-hydrido)-1,1,1,1,2,2,2,3,3,3-decacarbonyl-triangulo-triosmium)-1'-acetylferrocene

Guidance literature:: aluminium trichloride; In tetrachloromethane; (Ar); addn. of a soln. of osmium complex in CCl4 to a suspn. of AlCl3 and a soln. of CH3COCl in CCl4 at -15°C over 2 h with stirring, warming to 20°C; addn. of H2O, sepn., washing org. layer with ether, drying (CaCl2), concn., thin layer chromy. (SiO2, hexane/ether 4:1);
DOI:10.1023/A:1015064419785