C₁₇H₁₆INO

Base Information

Chemical Name:C₁₇H₁₆INO
CAS No.:1392323-53-3
Molecular Formula:C₁₇H₁₆INO
Molecular Weight:377.225
Hs Code.:

Synonyms:C₁₇H₁₆INO

Suppliers and Price of C₁₇H₁₆INO

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 0 raw suppliers

Chemical Property of C₁₇H₁₆INO

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of C₁₇H₁₆INO

There total 4 articles about C₁₇H₁₆INO which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 74.0%

: 1392323-05-5
N-(2-(but-1-en-2-yl)phenyl)benzamide

: 1392323-53-3
C₁₇H₁₆INO

Guidance literature:: With 3BF₄^(1-)*C₃₆H₅₈IN₄⁽³⁺⁾; (Ra)-4-hydroxy-2,6-bis(2,4,6-triisopropylphenyl)-9,14-bis(triisopropylsilyl)dinaphtho[1,3,2]dioxaphosphepine 4-oxide; sodium phosphate; In hexane; para-xylene; at 20 ℃; for 16h; optical yield given as %ee; enantioselective reaction; Inert atmosphere;
DOI:10.1021/ja305795x

Reference yield:

: 1196-28-7
2'-Aminopropiophenon

: 1392323-53-3
C₁₇H₁₆INO

Guidance literature:: Multi-step reaction with 3 steps

1.1: triethylamine / dichloromethane / 0.5 h / Inert atmosphere

2.1: sodium t-butanolate / diethyl ether / 0.5 h / 0 °C / Inert atmosphere

2.2: Reflux; Inert atmosphere

3.1: 3BF₄^(1-)*C₃₆H₅₈IN₄⁽³⁺⁾; (Ra)-4-hydroxy-2,6-bis(2,4,6-triisopropylphenyl)-9,14-bis(triisopropylsilyl)dinaphtho[1,3,2]dioxaphosphepine 4-oxide; sodium phosphate / hexane; para-xylene / 16 h / 20 °C / Inert atmosphere

With 3BF₄^(1-)*C₃₆H₅₈IN₄⁽³⁺⁾; (Ra)-4-hydroxy-2,6-bis(2,4,6-triisopropylphenyl)-9,14-bis(triisopropylsilyl)dinaphtho[1,3,2]dioxaphosphepine 4-oxide; triethylamine; sodium phosphate; sodium t-butanolate; In diethyl ether; hexane; dichloromethane; para-xylene; 2.2: Wittig reaction;
DOI:10.1021/ja305795x

Reference yield:

: 1885-29-6
anthranilic acid nitrile

: 1392323-53-3
C₁₇H₁₆INO

Guidance literature:: Multi-step reaction with 4 steps

1.1: diethyl ether / 0 - 20 °C / Inert atmosphere

2.1: triethylamine / dichloromethane / 0.5 h / Inert atmosphere

3.1: sodium t-butanolate / diethyl ether / 0.5 h / 0 °C / Inert atmosphere

3.2: Reflux; Inert atmosphere

4.1: 3BF₄^(1-)*C₃₆H₅₈IN₄⁽³⁺⁾; (Ra)-4-hydroxy-2,6-bis(2,4,6-triisopropylphenyl)-9,14-bis(triisopropylsilyl)dinaphtho[1,3,2]dioxaphosphepine 4-oxide; sodium phosphate / hexane; para-xylene / 16 h / 20 °C / Inert atmosphere

With 3BF₄^(1-)*C₃₆H₅₈IN₄⁽³⁺⁾; (Ra)-4-hydroxy-2,6-bis(2,4,6-triisopropylphenyl)-9,14-bis(triisopropylsilyl)dinaphtho[1,3,2]dioxaphosphepine 4-oxide; triethylamine; sodium phosphate; sodium t-butanolate; In diethyl ether; hexane; dichloromethane; para-xylene; 3.2: Wittig reaction;
DOI:10.1021/ja305795x