C₁₁H₆Cl₂N₂O₂

Base Information

Chemical Name:C₁₁H₆Cl₂N₂O₂
CAS No.:845752-02-5
Molecular Formula:C₁₁H₆Cl₂N₂O₂
Molecular Weight:269.087
Hs Code.:

C<sub>11</sub>H<sub>6</sub>Cl<sub>2</sub>N<sub>2</sub>O<sub>2</sub>

Synonyms:C₁₁H₆Cl₂N₂O₂

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Chemical Property of C₁₁H₆Cl₂N₂O₂

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Technology Process of C₁₁H₆Cl₂N₂O₂

There total 1 articles about C₁₁H₆Cl₂N₂O₂ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 52.0%

: 13091-23-1
4-chloro-3-nitropyridine

: 68716-47-2
2,4-dichlorophenylboronic acid

: 845752-02-5
C₁₁H₆Cl₂N₂O₂

Guidance literature:: With dipotassium hydrogenphosphate; tetrakis(triphenylphosphine) palladium⁽⁰⁾; In DMF (N,N-dimethyl-formamide); water; at 68 ℃; for 21h;

Reference yield: 83.0%

: 845752-02-5
C₁₁H₆Cl₂N₂O₂

: 845752-03-6
C₁₁H₈Cl₂N₂

Guidance literature:: With hydrogenchloride; iron; In ethanol; water; at 90 ℃; for 2h;

Reference yield:

: 845752-02-5
C₁₁H₆Cl₂N₂O₂

: 7-(2,4-dichloro-phenyl)-2-methyl-2H-pyrazolo[4,3-b]pyridine

Guidance literature:: Multi-step reaction with 9 steps

1.1: hydrogenchloride; iron / ethanol; water / 2 h / 90 °C

2.1: bromine; acetic acid / 23 h / 20 °C

3.1: methanesulfonic acid / 130 °C

4.1: hydrogen / palladium 10% on activated carbon / tetrahydrofuran; methanol / 8 h / 20 °C

5.1: pyrrolidine / ethanol / 0.25 h

6.1: potassium carbonate / (1,1'-bis(diphenylphosphino)ferrocene)palladium(II) dichloride / 1,4-dioxane; water / 2.5 h / 93 °C

7.1: potassium acetate; acetic anhydride / 14.5 h / 79 °C

8.1: lithium hydroxide; ethanol; water / 3 h / 79 °C

9.1: sodium hydride / tetrahydrofuran / 0.25 h / 0 °C

9.2: 0.5 h

With pyrrolidine; hydrogenchloride; lithium hydroxide; methanesulfonic acid; ethanol; water; hydrogen; bromine; potassium acetate; acetic anhydride; iron; sodium hydride; potassium carbonate; acetic acid; (1,1'-bis(diphenylphosphino)ferrocene)palladium(II) dichloride; palladium 10% on activated carbon; In tetrahydrofuran; 1,4-dioxane; methanol; ethanol; water;