6-[4-(4-benzylphthalazin-1-yl)piperazin-1-yl]pyridine-3-sulfonic acid amide

Base Information

Chemical Name:6-[4-(4-benzylphthalazin-1-yl)piperazin-1-yl]pyridine-3-sulfonic acid amide
CAS No.:1057677-68-5
Molecular Formula:C₂₄H₂₄N₆O₂S
Molecular Weight:460.56
Hs Code.:

Synonyms:6-[4-(4-benzylphthalazin-1-yl)piperazin-1-yl]pyridine-3-sulfonic acid amide

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Chemical Property of 6-[4-(4-benzylphthalazin-1-yl)piperazin-1-yl]pyridine-3-sulfonic acid amide

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Technology Process of 6-[4-(4-benzylphthalazin-1-yl)piperazin-1-yl]pyridine-3-sulfonic acid amide

There total 2 articles about 6-[4-(4-benzylphthalazin-1-yl)piperazin-1-yl]pyridine-3-sulfonic acid amide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 30.0%

: 40741-46-6
6-chloro-pyridine-3-sulfonic acid amide

: 1-(piperazin-1-yl)-4-benzylphthalazine

: 1057677-68-5
6-[4-(4-benzylphthalazin-1-yl)piperazin-1-yl]pyridine-3-sulfonic acid amide

Guidance literature:: With triethylamine; In 1-methyl-pyrrolidin-2-one; at 180 ℃; for 0.5h; Microwave irradiation; Inert atmosphere;
DOI:10.1021/jm900309j

Reference yield:

: 1057677-68-5
6-[4-(4-benzylphthalazin-1-yl)piperazin-1-yl]pyridine-3-sulfonic acid amide

Guidance literature:

Reference yield: 77.0%

: 1057677-68-5
6-[4-(4-benzylphthalazin-1-yl)piperazin-1-yl]pyridine-3-sulfonic acid amide

: 107-21-1
ethylene glycol

: 1057678-80-4
1-benzyl-4-(4-(5-(2-methyl-1,3-dioxolan-2-yl)pyridin-2-yl)piperazin-1-yl)phthalazine

Guidance literature:: 6-[4-(4-benzylphthalazin-1-yl)piperazin-1-yl]pyridine-3-sulfonic acid amide; ethylene glycol; With toluene-4-sulfonic acid; In toluene; for 48h; Heating / reflux;

With sodium hydrogencarbonate; In dichloromethane; water; toluene;