(E)-trimethyl[5-phenyl-1-(4-trifluoromethylphenyl)-2-penten-1-yl]silane

Base Information

• Chemical Name: (E)-trimethyl[5-phenyl-1-(4-trifluoromethylphenyl)-2-penten-1-yl]silane
• CAS No.: 1237538-52-1
• Molecular Formula: C₂₁H₂₅F₃Si
• Molecular Weight: 362.51
• Mol file: 1237538-52-1.mol

Synonyms:(E)-trimethyl[5-phenyl-1-(4-trifluoromethylphenyl)-2-penten-1-yl]silane

Chemical Property of (E)-trimethyl[5-phenyl-1-(4-trifluoromethylphenyl)-2-penten-1-yl]silane

Chemical Property:

Purity/Quality:

Safty Information:

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Technology Process of (E)-trimethyl[5-phenyl-1-(4-trifluoromethylphenyl)-2-penten-1-yl]silane

There total 2 articles about (E)-trimethyl[5-phenyl-1-(4-trifluoromethylphenyl)-2-penten-1-yl]silane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 82.0%

(E)-5-phenyl-1-trimethylsilyl-1-penten-3-yl 2-methoxybenzoate (1237539-30-8) + 4-trifluoromethylphenylboronic acid (128796-39-4) → (E)-trimethyl[5-phenyl-1-(4-trifluoromethylphenyl)-2-penten-1-yl]silane (1237538-52-1) + C26H23F3O3

Guidance literature:

With silver hexafluoroantimonate; 1,10-Phenanthroline; palladium diacetate; p-benzoquinone; In 1,2-dichloro-ethane; at 25 - 60 ℃; regioselective reaction;

DOI:10.1021/ol101114r

Reference yield: 45.0%

(E)-5-phenyl-1-trimethylsilyl-1-penten-3-yl 2-methoxybenzoate (1237539-30-8) + 4-trifluoromethylphenylboronic acid (128796-39-4) → (E)-trimethyl[5-phenyl-1-(4-trifluoromethylphenyl)-2-penten-1-yl]silane (1237538-52-1)

Guidance literature:

With silver hexafluoroantimonate; bathophenanthroline; palladium diacetate; In tetrahydrofuran; at 25 - 60 ℃; regioselective reaction;

DOI:10.1021/ol101114r

upstream raw materials:

(E)-5-phenyl-1-trimethylsilyl-1-penten-3-yl 2-methoxybenzoate

4-trifluoromethylphenylboronic acid