thioacetic acid S-[10-(2-formyl-phenylcarbamoyl)-decyl] ester

Base Information

• Chemical Name: thioacetic acid S-[10-(2-formyl-phenylcarbamoyl)-decyl] ester
• CAS No.: 240813-42-7
• Molecular Formula: C₂₀H₂₉NO₃S
• Molecular Weight: 363.521
• Mol file: 240813-42-7.mol

Synonyms:thioacetic acid S-[10-(2-formyl-phenylcarbamoyl)-decyl] ester

Chemical Property of thioacetic acid S-[10-(2-formyl-phenylcarbamoyl)-decyl] ester

Chemical Property:

Purity/Quality:

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MSDS Files:

Useful:

Technology Process of thioacetic acid S-[10-(2-formyl-phenylcarbamoyl)-decyl] ester

There total 5 articles about thioacetic acid S-[10-(2-formyl-phenylcarbamoyl)-decyl] ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 80.0%

11-bromo-undecanoic acid (2-formyl-phenyl)-amide (240813-39-2) + potassium thioacetate (10387-40-3) → thioacetic acid S-[10-(2-formyl-phenylcarbamoyl)-decyl] ester (240813-42-7)

Guidance literature:

DOI:10.1039/a809918i

Reference yield:

5,5-Dimethyl-2-(2-nitro-phenyl)-[1,3]dioxane (79718-94-8) → thioacetic acid S-[10-(2-formyl-phenylcarbamoyl)-decyl] ester (240813-42-7)

Guidance literature:

Multi-step reaction with 4 steps

1: 72 percent / H₂ / Pd/C

2: 99 percent / N-methylmorpholine, 2-chloro-4,6-dimethoxy-1,3,5-triazine

3: 99 percent / H₂SO₄, TFA

4: 80 percent

With 4-methyl-morpholine; 2-chloro-4,6-dimethoxy-1 ,3,5-triazine; sulfuric acid; hydrogen; trifluoroacetic acid; palladium on activated charcoal;

DOI:10.1039/a809918i

Reference yield:

2-nitro-benzaldehyde (552-89-6) → thioacetic acid S-[10-(2-formyl-phenylcarbamoyl)-decyl] ester (240813-42-7)

Guidance literature:

Multi-step reaction with 5 steps

1: 91 percent / TsOH

2: 72 percent / H₂ / Pd/C

3: 99 percent / N-methylmorpholine, 2-chloro-4,6-dimethoxy-1,3,5-triazine

4: 99 percent / H₂SO₄, TFA

5: 80 percent

With 4-methyl-morpholine; 2-chloro-4,6-dimethoxy-1 ,3,5-triazine; sulfuric acid; hydrogen; toluene-4-sulfonic acid; trifluoroacetic acid; palladium on activated charcoal;

DOI:10.1039/a809918i

upstream raw materials:

11-bromo-undecanoic acid (2-formyl-phenyl)-amide

potassium thioacetate

5,5-Dimethyl-2-(2-nitro-phenyl)-[1,3]dioxane

2-nitro-benzaldehyde

Downstream raw materials:

11-mercapto-undecanoic acid (2-formyl-phenyl)-amide