HCOC₆H₄N(CH₂CH₂SCH₂COOCH₃)2

Base Information

• Chemical Name: HCOC₆H₄N(CH₂CH₂SCH₂COOCH₃)2
• CAS No.: 1202206-37-8
• Molecular Formula: C₁₇H₂₃NO₅S₂
• Molecular Weight: 385.505
• Mol file: 1202206-37-8.mol

Synonyms:HCOC₆H₄N(CH₂CH₂SCH₂COOCH₃)2

Chemical Property of HCOC₆H₄N(CH₂CH₂SCH₂COOCH₃)2

Chemical Property:

Purity/Quality:

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MSDS Files:

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Technology Process of HCOC₆H₄N(CH₂CH₂SCH₂COOCH₃)2

There total 1 articles about HCOC₆H₄N(CH₂CH₂SCH₂COOCH₃)2 which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 60.0%

C16H23NO4S2 (1202206-35-6) → HCOC6H4N(CH2CH2SCH2COOCH3)2 (1202206-37-8)

Guidance literature:

With trichlorophosphate; In N,N-dimethyl-formamide; at 0 - 20 ℃; Inert atmosphere;

DOI:10.1021/ja906500m

Reference yield: 40.0%

HCOC6H4N(CH2CH2SCH2COOCH3)2 (1202206-37-8) + BODIPY → BF2(C4HN(CH3))2CH3CC6H4O(CH2CH2O)3CH3CHCHC6H4N(CH2CH2SCH2CO2CH3)2 (1357927-62-8)

Guidance literature:

With piperidine; In acetic acid; toluene; (under N2); mixt. of B-compound, ligand, CH3CO2H, piperidine and toluenerefluxed; H2O removed azeotropically over 30 min, volatiles removed in vacuo, silica gel column chromy. with CHCl3, exclusion chromy. with THF;

DOI:10.1039/c1dt11546d

Reference yield: 38.0%

2,4-dimethyl-1H-pyrrole (625-82-1) + HCOC6H4N(CH2CH2SCH2COOCH3)2 (1202206-37-8) → F2B(C4H(CH3)2N)2CC6H4N(CH2CH2SCH2COOCH3)2 (1202380-86-6)

Guidance literature:

2,4-dimethyl-1H-pyrrole; HCOC₆H₄N(CH₂CH₂SCH₂COOCH₃)2; With trifluoroacetic acid; In dichloromethane; at 20 ℃; for 1.5h; Inert atmosphere; Darkness;

With 2,3-dicyano-5,6-dichloro-p-benzoquinone; In dichloromethane; for 1h; Further stages; Inert atmosphere;

DOI:10.1021/ja906500m

upstream raw materials:

C₁₆H₂₃NO₄S₂

Downstream raw materials:

F₂B(C₄H(CH₃)2N)2CC₆H₄N(CH₂CH₂SCH₂COOCH₃)2

BF₂(C₄HN(CH₃))2CH₃CC₆H₄O(CH₂CH₂O)3CH₃CHCHC₆H₄N(CH₂CH₂SCH₂CO₂CH₃)2