4-Methylbrenzcatechin-2-O-triacetyl-β-D-glucopyranosiduronsaeuremethylester

Base Information

Chemical Name:4-Methylbrenzcatechin-2-O-triacetyl-β-D-glucopyranosiduronsaeuremethylester
CAS No.:117591-57-8
Molecular Formula:C₂₀H₂₄O₁₁
Molecular Weight:440.404
Hs Code.:

Synonyms:4-Methylbrenzcatechin-2-O-triacetyl-β-D-glucopyranosiduronsaeuremethylester

Suppliers and Price of 4-Methylbrenzcatechin-2-O-triacetyl-β-D-glucopyranosiduronsaeuremethylester

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 4-Methylbrenzcatechin-2-O-triacetyl-β-D-glucopyranosiduronsaeuremethylester

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Technology Process of 4-Methylbrenzcatechin-2-O-triacetyl-β-D-glucopyranosiduronsaeuremethylester

There total 2 articles about 4-Methylbrenzcatechin-2-O-triacetyl-β-D-glucopyranosiduronsaeuremethylester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 24.0%

: 452-86-8
4-methyl-1,2-dihydroxybenzene

: 7355-18-2
(2S,3S,4S,5R,6S)-3,4,5,6-Tetraacetoxy-tetrahydro-pyran-2-carboxylic acid methyl ester

: 117591-57-8
4-Methylbrenzcatechin-2-O-triacetyl-β-D-glucopyranosiduronsaeuremethylester

Guidance literature:: With toluene-4-sulfonic acid; at 100 - 110 ℃; for 0.75h; under 3 - 6 Torr;

Reference yield:

: 92420-89-8
methyl 2,3,4-tri-O-acetyl-1-O-(trichloroacetimidoyl)-α-D-glucopyranuronate

: 452-86-8
4-methyl-1,2-dihydroxybenzene

: methyl 2,3,4-tri-O-acetyl-1-O-(2-hydroxy-4-methylphenyl)-β-D-glucuronate

: 117591-57-8
4-Methylbrenzcatechin-2-O-triacetyl-β-D-glucopyranosiduronsaeuremethylester

Guidance literature:: With boron trifluoride diethyl etherate; In dichloromethane; at -20 - 20 ℃; for 4h; Overall yield = 38 %; Overall yield = 177 mg; Inert atmosphere; Molecular sieve;
DOI:10.1021/acs.jafc.6b05629