2-hydroxy-5-methylphenyl beta-D-glucopyranosiduronic acid

Base Information

Chemical Name:2-hydroxy-5-methylphenyl beta-D-glucopyranosiduronic acid
CAS No.:117591-51-2
Molecular Formula:C13H16 O8
Molecular Weight:300.2613
Hs Code.:

Synonyms:

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Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 2-hydroxy-5-methylphenyl beta-D-glucopyranosiduronic acid

Chemical Property:

Vapor Pressure:2.7E-15mmHg at 25°C
Boiling Point:601°C at 760 mmHg
Flash Point:230.6°C
Density:1.623g/cm³

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Technology Process of 2-hydroxy-5-methylphenyl beta-D-glucopyranosiduronic acid

There total 4 articles about 2-hydroxy-5-methylphenyl beta-D-glucopyranosiduronic acid which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 90.0%

: 117591-57-8
4-Methylbrenzcatechin-2-O-triacetyl-β-D-glucopyranosiduronsaeuremethylester

: 117591-51-2
4-Methylbrenzcatechin-2-O-β-D-glucopyranosiduronsaeure

Guidance literature:: With sodium hydroxide; In water; for 0.5h;

Reference yield:

: 92420-89-8
methyl 2,3,4-tri-O-acetyl-1-O-(trichloroacetimidoyl)-α-D-glucopyranuronate

: 452-86-8
4-methyl-1,2-dihydroxybenzene

: 1-O-(2-hydroxy-4-methylphenyl)-β-D-glucuronic acid

: 117591-51-2
4-Methylbrenzcatechin-2-O-β-D-glucopyranosiduronsaeure

Guidance literature:: methyl 2,3,4-tri-O-acetyl-1-O-(trichloroacetimidoyl)-α-D-glucopyranuronate; 4-methyl-1,2-dihydroxybenzene; With boron trifluoride diethyl etherate; In dichloromethane; at -20 - 20 ℃; for 4h; Inert atmosphere; Molecular sieve;

With sodium methylate; In methanol; at 20 ℃; for 0.25h; Inert atmosphere;

With lithium hydroxide; In water; at 20 ℃; for 0.0833333h; Overall yield = 62 mg;
DOI:10.1021/acs.jafc.6b05629

Reference yield:

: 452-86-8
4-methyl-1,2-dihydroxybenzene

: 117591-51-2
4-Methylbrenzcatechin-2-O-β-D-glucopyranosiduronsaeure

Guidance literature:: Multi-step reaction with 2 steps

1: 24 percent / TsOH*H₂O / 0.75 h / 100 - 110 °C / 3 - 6 Torr

2: 90 percent / NaOH / H₂O / 0.5 h

With sodium hydroxide; toluene-4-sulfonic acid; In water;