N-(2,2,2-trifluoro-ethyl)-2-fluoro-4-methylamino-5-nitro-benzoic acid amide

Base Information

Chemical Name:N-(2,2,2-trifluoro-ethyl)-2-fluoro-4-methylamino-5-nitro-benzoic acid amide
CAS No.:1380837-08-0
Molecular Formula:C₁₀H₉F₄N₃O₃
Molecular Weight:295.193
Hs Code.:

Synonyms:N-(2,2,2-trifluoro-ethyl)-2-fluoro-4-methylamino-5-nitro-benzoic acid amide

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Chemical Property of N-(2,2,2-trifluoro-ethyl)-2-fluoro-4-methylamino-5-nitro-benzoic acid amide

Chemical Property:

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Technology Process of N-(2,2,2-trifluoro-ethyl)-2-fluoro-4-methylamino-5-nitro-benzoic acid amide

There total 1 articles about N-(2,2,2-trifluoro-ethyl)-2-fluoro-4-methylamino-5-nitro-benzoic acid amide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1380837-08-0
N-(2,2,2-trifluoro-ethyl)-2-fluoro-4-methylamino-5-nitro-benzoic acid amide

Guidance literature:

Reference yield:

: 22990-34-7
2-(piperidin-4-yl)propan-2-ol

: 1380837-08-0
N-(2,2,2-trifluoro-ethyl)-2-fluoro-4-methylamino-5-nitro-benzoic acid amide

: 1380836-23-6
N-(2,2,2-trifluoroethyl)-2-[4-(1-hydroxy-1-methyl-ethyl)-piperidinyl]-4-methylamino-5-nitro-benzoic acid amide

Guidance literature:: 2-(piperidin-4-yl)propan-2-ol; With sodium hydride; In tetrahydrofuran; mineral oil; for 0.166667h;

N-(2,2,2-trifluoro-ethyl)-2-fluoro-4-methylamino-5-nitro-benzoic acid amide; In tetrahydrofuran; mineral oil; for 1.5h;

Reference yield:

: 22990-34-7
2-(piperidin-4-yl)propan-2-ol

: 1380837-08-0
N-(2,2,2-trifluoro-ethyl)-2-fluoro-4-methylamino-5-nitro-benzoic acid amide

: 1380836-25-8
N-(2,2,2-Trifluoroethyl)-2-[4-(1-hydroxy-1-methyl-ethyl)-piperidinyl]-4-methylamino-5-amino-benzoic acid amide

Guidance literature:: Multi-step reaction with 2 steps

1.1: sodium hydride / tetrahydrofuran; mineral oil / 0.17 h

1.2: 1.5 h

2.1: hydrogen / palladium on activated charcoal / tetrahydrofuran; methanol / 7 h / 2250.23 Torr

With hydrogen; sodium hydride; palladium on activated charcoal; In tetrahydrofuran; methanol; mineral oil;