C₁₇H₈⁽²⁾H₆N₂O

Base Information

• Chemical Name: C₁₇H₈⁽²⁾H₆N₂O
• CAS No.: 1428858-73-4
• Molecular Formula: C₁₇H₁₄N₂O
• Molecular Weight: 268.263
• Mol file: 1428858-73-4.mol

Synonyms:C₁₇H₈⁽²⁾H₆N₂O

Chemical Property of C₁₇H₈⁽²⁾H₆N₂O

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
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MSDS Files:

Useful:

Technology Process of C₁₇H₈⁽²⁾H₆N₂O

There total 7 articles about C₁₇H₈⁽²⁾H₆N₂O which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 74.0%

ortho-nitrobenzoic acid (552-16-9,104810-18-6) + 2-[(2)H3]-methyl-N-(8-quinolinyl)-[(2)H5]-benzamide (1351066-84-6) → C17H8(2)H6N2O (1428858-73-4) + 3-methyl-2'-nitro-N-(quinolin-8-yl)-(1,1'-biphenyl)-2-carboxamide

Guidance literature:

With copper(II) acetate monohydrate; In dimethyl sulfoxide; at 100 ℃; for 4h;

DOI:10.1002/anie.201701918

Reference yield: 56.0%

2-[(2)H3]-methyl-N-(8-quinolinyl)-[(2)H5]-benzamide (1351066-84-6) → C17H8(2)H6N2O (1428858-73-4)

Guidance literature:

With tris(triphenylphosphine)ruthenium(II) chloride; sodium acetate; In toluene; at 100 ℃; for 4h;

DOI:10.1039/c3sc50310k

Reference yield: 42.0%

ortho-nitrobenzoic acid (552-16-9,104810-18-6) + 2-[(2)H3]-methyl-N-(8-quinolinyl)-[(2)H5]-benzamide (1351066-84-6) → C17H8(2)H6N2O (1428858-73-4)

Guidance literature:

With copper(II) acetate monohydrate; In dimethyl sulfoxide; at 100 ℃; for 4h;

DOI:10.1002/anie.201701918

upstream raw materials:

bromobenzene

2-[(2)H3]-methyl-N-(8-quinolinyl)-[(2)H5]-benzamide

methyl vinyl ketone

1-bromo-butane

Downstream raw materials:

2-[(2)H3]-methyl-N-(8-quinolinyl)-[(2)H5]-benzamide