2-({[tert-butyl(dimethyl)silyl]oxy}methyl)-2-phenyl-4-(triisopropylsilyl)-3-butynal

Base Information

Chemical Name:2-({[tert-butyl(dimethyl)silyl]oxy}methyl)-2-phenyl-4-(triisopropylsilyl)-3-butynal
CAS No.:1229626-49-6
Molecular Formula:C₂₆H₄₄O₂Si₂
Molecular Weight:444.805
Hs Code.:

Synonyms:2-({[tert-butyl(dimethyl)silyl]oxy}methyl)-2-phenyl-4-(triisopropylsilyl)-3-butynal

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 2-({[tert-butyl(dimethyl)silyl]oxy}methyl)-2-phenyl-4-(triisopropylsilyl)-3-butynal

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Technology Process of 2-({[tert-butyl(dimethyl)silyl]oxy}methyl)-2-phenyl-4-(triisopropylsilyl)-3-butynal

There total 1 articles about 2-({[tert-butyl(dimethyl)silyl]oxy}methyl)-2-phenyl-4-(triisopropylsilyl)-3-butynal which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 67.0%

: tert-butyl(dimethyl)({3-phenyl-3-[(triisopropylsilyl)ethynyl]-2-oxiranyl}methoxy)silane

: 1229626-49-6
2-({[tert-butyl(dimethyl)silyl]oxy}methyl)-2-phenyl-4-(triisopropylsilyl)-3-butynal

Guidance literature:: With 4-bromo-2,6-di-tert-butylphenol; trimethylaluminum; In n-heptane; dichloromethane; at -78 ℃;
DOI:10.1002/ejoc.201000076

Reference yield: 93.0%

: 558-13-4
carbon tetrabromide

: 1229626-49-6
2-({[tert-butyl(dimethyl)silyl]oxy}methyl)-2-phenyl-4-(triisopropylsilyl)-3-butynal

: 1229626-50-9
tert-butyl({4,4-dibromo-2-phenyl-2-[(triisopropylsilyl)ethynyl]-3-buten-1-yl}oxy)dimethylsilane

Guidance literature:: carbon tetrabromide; With triphenylphosphine; In dichloromethane; at 0 ℃; for 0.25h;

2-({[tert-butyl(dimethyl)silyl]oxy}methyl)-2-phenyl-4-(triisopropylsilyl)-3-butynal; In dichloromethane; at 0 ℃; for 3h;
DOI:10.1002/ejoc.201000076