N-(2-bromo-4-methoxyphenyl)-N-(cyclopropylmethyl)-1,1,1-trifluoromethanesulfonamide

Base Information

Chemical Name:N-(2-bromo-4-methoxyphenyl)-N-(cyclopropylmethyl)-1,1,1-trifluoromethanesulfonamide
CAS No.:1426327-90-3
Molecular Formula:C₁₂H₁₃BrF₃NO₃S
Molecular Weight:388.205
Hs Code.:

Synonyms:N-(2-bromo-4-methoxyphenyl)-N-(cyclopropylmethyl)-1,1,1-trifluoromethanesulfonamide

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Chemical Property of N-(2-bromo-4-methoxyphenyl)-N-(cyclopropylmethyl)-1,1,1-trifluoromethanesulfonamide

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Technology Process of N-(2-bromo-4-methoxyphenyl)-N-(cyclopropylmethyl)-1,1,1-trifluoromethanesulfonamide

There total 2 articles about N-(2-bromo-4-methoxyphenyl)-N-(cyclopropylmethyl)-1,1,1-trifluoromethanesulfonamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 358-23-6
trifluoromethylsulfonic anhydride

: C₁₁H₁₄BrNO

: 1426327-90-3
N-(2-bromo-4-methoxyphenyl)-N-(cyclopropylmethyl)-1,1,1-trifluoromethanesulfonamide

Guidance literature:: C₁₁H₁₄BrNO; With sodium hydride; In 1,2-dichloro-ethane; at 0 ℃; Inert atmosphere;

trifluoromethylsulfonic anhydride; In 1,2-dichloro-ethane; at 0 - 20 ℃; Inert atmosphere;
DOI:10.1021/ol400380y

Reference yield:

: 316790-75-7
cyclopropanecarboxylic acid (2-bromo-4-methoxy-phenyl)-amide

: 1426327-90-3
N-(2-bromo-4-methoxyphenyl)-N-(cyclopropylmethyl)-1,1,1-trifluoromethanesulfonamide

Guidance literature:: Multi-step reaction with 2 steps

1.1: diborane / tetrahydrofuran / 8 h / Inert atmosphere; Reflux

2.1: sodium hydride / 1,2-dichloro-ethane / 0 °C / Inert atmosphere

2.2: 0 - 20 °C / Inert atmosphere

With sodium hydride; diborane; In tetrahydrofuran; 1,2-dichloro-ethane;
DOI:10.1021/ol400380y