Technology Process of (+)-3,3-ethylenedithio-2-phenyl-1-phthalimidobutane
There total 7 articles about (+)-3,3-ethylenedithio-2-phenyl-1-phthalimidobutane which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
With
boron trifluoride diethyl etherate;
In
diethyl ether;
1.) -10 deg C, 1 h, 2.) room temperature, 3 days;
DOI:10.1039/P19810000906
- Guidance literature:
-
Multi-step reaction with 5 steps
1: 85 percent / triethylamine / toluene / 5 h / Heating
2: 97 percent / thionyl chloride / 5 h / Heating
3: 90 percent / diethyl ether; benzene / 12 h / 20 °C
4: 85 percent / 67percent hydriodic acid / CHCl3 / 0.33 h / -5 °C
5: 81 percent / boron trifluoride-ether / diethyl ether / 1.) -10 deg C, 1 h, 2.) room temperature, 3 days
With
thionyl chloride; boron trifluoride diethyl etherate; hydrogen iodide; triethylamine;
In
diethyl ether; chloroform; toluene; benzene;
DOI:10.1039/P19810000906
- Guidance literature:
-
Multi-step reaction with 6 steps
2: 85 percent / triethylamine / toluene / 5 h / Heating
3: 97 percent / thionyl chloride / 5 h / Heating
4: 90 percent / diethyl ether; benzene / 12 h / 20 °C
5: 85 percent / 67percent hydriodic acid / CHCl3 / 0.33 h / -5 °C
6: 81 percent / boron trifluoride-ether / diethyl ether / 1.) -10 deg C, 1 h, 2.) room temperature, 3 days
With
thionyl chloride; boron trifluoride diethyl etherate; hydrogen iodide; triethylamine;
In
diethyl ether; chloroform; toluene; benzene;
DOI:10.1039/P19810000906
