2,6,7-Trideoxy-7-C-(2,4-dichlorophenyl)-3,4,5-tri-O-(4-methoxybenzyl)-D-xylo-heptonamide

Base Information

Chemical Name:2,6,7-Trideoxy-7-C-(2,4-dichlorophenyl)-3,4,5-tri-O-(4-methoxybenzyl)-D-xylo-heptonamide
CAS No.:141240-39-3
Molecular Formula:C₃₇H₄₁Cl₂NO₇
Molecular Weight:682.641
Hs Code.:

Synonyms:2,6,7-Trideoxy-7-C-(2,4-dichlorophenyl)-3,4,5-tri-O-(4-methoxybenzyl)-D-xylo-heptonamide

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Chemical Property of 2,6,7-Trideoxy-7-C-(2,4-dichlorophenyl)-3,4,5-tri-O-(4-methoxybenzyl)-D-xylo-heptonamide

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Technology Process of 2,6,7-Trideoxy-7-C-(2,4-dichlorophenyl)-3,4,5-tri-O-(4-methoxybenzyl)-D-xylo-heptonamide

There total 6 articles about 2,6,7-Trideoxy-7-C-(2,4-dichlorophenyl)-3,4,5-tri-O-(4-methoxybenzyl)-D-xylo-heptonamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 38.0%

: 141240-41-7
2,6,7-Trideoxy-7-C-(2,4-dichlorophenyl)-3,4,5-tri-O-(4-methoxybenzyl)-D-xylo-heptonitrile

: 141240-27-9
1,4-Anhydro-2,3-di-O-benzyl-5,6-dideoxy-6-C-(2,4-dichlorophenyl)-D-xylo-hexitol

: 141240-39-3
2,6,7-Trideoxy-7-C-(2,4-dichlorophenyl)-3,4,5-tri-O-(4-methoxybenzyl)-D-xylo-heptonamide

Guidance literature:: With dihydrogen peroxide; potassium carbonate; In dimethyl sulfoxide; Ambient temperature;
DOI:10.1016/S0008-6215(00)90499-3

Reference yield:

: 141240-05-3,141317-09-1
(Z)-1,3-di-O-acetyl-2,4-O-benzylidene-5,6-dideoxy-6-C-(2,4-dichlorophenyl)-D-xylo-hex-5-enitol

: 141240-39-3
2,6,7-Trideoxy-7-C-(2,4-dichlorophenyl)-3,4,5-tri-O-(4-methoxybenzyl)-D-xylo-heptonamide

Guidance literature:: Multi-step reaction with 6 steps

1: 1) H₂, 2) 4M NaOMe / 1) 10percent Pd / C / 1) r.t., 2.5 h, 2) methanol, r.t., 1 h

2: 93 percent / pyridine / 72 h / Ambient temperature

3: 1) NaH, Me₂SO / 1) DMSO, 30 min., r.t, 2) DMSO, 2 h, r.t.

4: 78 percent / 2M HCl / CHCl₃; methanol / 48 h / 4 °C

5: 37 percent / triphenylphosphine, diethyl azodicarboxylate / benzene / Ambient temperature

6: 68.8 percent / K₂CO₃, 30percent H₂O₂ / dimethylsulfoxide / Ambient temperature

With pyridine; hydrogenchloride; hydrogen; dihydrogen peroxide; sodium methylate; sodium hydride; potassium carbonate; dimethyl sulfoxide; triphenylphosphine; diethylazodicarboxylate; palladium on activated charcoal; In methanol; chloroform; dimethyl sulfoxide; benzene;
DOI:10.1016/S0008-6215(00)90499-3

Reference yield:

: 141240-23-5
5,6-Dideoxy-6-C-(2,4-dichlorophenyl)-1-O-trityl-D-xylo-hexitol

: 141240-39-3
2,6,7-Trideoxy-7-C-(2,4-dichlorophenyl)-3,4,5-tri-O-(4-methoxybenzyl)-D-xylo-heptonamide

Guidance literature:: Multi-step reaction with 4 steps

1: 1) NaH, Me₂SO / 1) DMSO, 30 min., r.t, 2) DMSO, 2 h, r.t.

2: 78 percent / 2M HCl / CHCl₃; methanol / 48 h / 4 °C

3: 37 percent / triphenylphosphine, diethyl azodicarboxylate / benzene / Ambient temperature

4: 68.8 percent / K₂CO₃, 30percent H₂O₂ / dimethylsulfoxide / Ambient temperature

With hydrogenchloride; dihydrogen peroxide; sodium hydride; potassium carbonate; dimethyl sulfoxide; triphenylphosphine; diethylazodicarboxylate; In methanol; chloroform; dimethyl sulfoxide; benzene;
DOI:10.1016/S0008-6215(00)90499-3