5,6-Dideoxy-6-C-(2,4-dichlorophenyl)-2,3,4-tri-O-(4-methoxybenzyl)-D-xylo-hexitol

Base Information

Chemical Name:5,6-Dideoxy-6-C-(2,4-dichlorophenyl)-2,3,4-tri-O-(4-methoxybenzyl)-D-xylo-hexitol
CAS No.:141240-36-0
Molecular Formula:C₃₆H₄₀Cl₂O₇
Molecular Weight:655.615
Hs Code.:

Synonyms:5,6-Dideoxy-6-C-(2,4-dichlorophenyl)-2,3,4-tri-O-(4-methoxybenzyl)-D-xylo-hexitol

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Chemical Property of 5,6-Dideoxy-6-C-(2,4-dichlorophenyl)-2,3,4-tri-O-(4-methoxybenzyl)-D-xylo-hexitol

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Technology Process of 5,6-Dideoxy-6-C-(2,4-dichlorophenyl)-2,3,4-tri-O-(4-methoxybenzyl)-D-xylo-hexitol

There total 4 articles about 5,6-Dideoxy-6-C-(2,4-dichlorophenyl)-2,3,4-tri-O-(4-methoxybenzyl)-D-xylo-hexitol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 78.0%

: 141240-26-8
5,6-Dideoxy-6-C-(2,4-dichlorophenyl)2,3,4-tri-O-(4-methoxybenzyl)-1-O-tri-phenylmethyl-D-xylo-hexitol

: 141240-36-0
5,6-Dideoxy-6-C-(2,4-dichlorophenyl)-2,3,4-tri-O-(4-methoxybenzyl)-D-xylo-hexitol

Guidance literature:: With hydrogenchloride; In methanol; chloroform; at 4 ℃; for 48h;
DOI:10.1016/S0008-6215(00)90499-3

Reference yield:

: 141240-05-3,141317-09-1
(Z)-1,3-di-O-acetyl-2,4-O-benzylidene-5,6-dideoxy-6-C-(2,4-dichlorophenyl)-D-xylo-hex-5-enitol

: 141240-36-0
5,6-Dideoxy-6-C-(2,4-dichlorophenyl)-2,3,4-tri-O-(4-methoxybenzyl)-D-xylo-hexitol

Guidance literature:: Multi-step reaction with 4 steps

1: 1) H₂, 2) 4M NaOMe / 1) 10percent Pd / C / 1) r.t., 2.5 h, 2) methanol, r.t., 1 h

2: 93 percent / pyridine / 72 h / Ambient temperature

3: 1) NaH, Me₂SO / 1) DMSO, 30 min., r.t, 2) DMSO, 2 h, r.t.

4: 78 percent / 2M HCl / CHCl₃; methanol / 48 h / 4 °C

With pyridine; hydrogenchloride; hydrogen; sodium methylate; sodium hydride; dimethyl sulfoxide; palladium on activated charcoal; In methanol; chloroform;
DOI:10.1016/S0008-6215(00)90499-3

Reference yield:

: 141240-23-5
5,6-Dideoxy-6-C-(2,4-dichlorophenyl)-1-O-trityl-D-xylo-hexitol

: 141240-36-0
5,6-Dideoxy-6-C-(2,4-dichlorophenyl)-2,3,4-tri-O-(4-methoxybenzyl)-D-xylo-hexitol

Guidance literature:: Multi-step reaction with 2 steps

1: 1) NaH, Me₂SO / 1) DMSO, 30 min., r.t, 2) DMSO, 2 h, r.t.

2: 78 percent / 2M HCl / CHCl₃; methanol / 48 h / 4 °C

With hydrogenchloride; sodium hydride; dimethyl sulfoxide; In methanol; chloroform;
DOI:10.1016/S0008-6215(00)90499-3