(4-[4-(tert-butoxycarbonylphenylamino)butoxysulfonyl]phenyl)acetic acid methyl ester

Base Information

Chemical Name:(4-[4-(tert-butoxycarbonylphenylamino)butoxysulfonyl]phenyl)acetic acid methyl ester
CAS No.:1425707-99-8
Molecular Formula:C₂₄H₃₁NO₇S
Molecular Weight:477.579
Hs Code.:

Synonyms:(4-[4-(tert-butoxycarbonylphenylamino)butoxysulfonyl]phenyl)acetic acid methyl ester

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Chemical Property of (4-[4-(tert-butoxycarbonylphenylamino)butoxysulfonyl]phenyl)acetic acid methyl ester

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Technology Process of (4-[4-(tert-butoxycarbonylphenylamino)butoxysulfonyl]phenyl)acetic acid methyl ester

There total 5 articles about (4-[4-(tert-butoxycarbonylphenylamino)butoxysulfonyl]phenyl)acetic acid methyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 83.0%

: 53305-12-7
2-(4-(chlorosulfonyl)phenyl)acetic acid methyl ester

: 1425707-85-2
(4-hydroxybutyl)phenylcarbamic acid tert-butyl ester

: 1425707-99-8
(4-[4-(tert-butoxycarbonylphenylamino)butoxysulfonyl]phenyl)acetic acid methyl ester

Guidance literature:: With dmap; triethylamine; In dichloromethane; at 20 ℃; for 3h; Inert atmosphere;
DOI:10.1002/chem.201202474

Reference yield:

: 101-41-7
benzeneacetic acid methyl ester

: 1425707-99-8
(4-[4-(tert-butoxycarbonylphenylamino)butoxysulfonyl]phenyl)acetic acid methyl ester

Guidance literature:: Multi-step reaction with 2 steps

1: chlorosulfonic acid / dichloromethane / 38 h / 0 - 20 °C / Inert atmosphere

2: triethylamine; dmap / dichloromethane / 3 h / 20 °C / Inert atmosphere

With chlorosulfonic acid; dmap; triethylamine; In dichloromethane;
DOI:10.1002/chem.201202474

Reference yield:

: 6517-80-2
4-(phenylamino)butan-1-ol

: 1425707-99-8
(4-[4-(tert-butoxycarbonylphenylamino)butoxysulfonyl]phenyl)acetic acid methyl ester

Guidance literature:: Multi-step reaction with 2 steps

1: sodium hydrogencarbonate / chloroform / Inert atmosphere; Reflux

2: triethylamine; dmap / dichloromethane / 3 h / 20 °C / Inert atmosphere

With dmap; sodium hydrogencarbonate; triethylamine; In dichloromethane; chloroform;
DOI:10.1002/chem.201202474