Carbonic acid (E)-(R)-1-benzyloxymethyl-3-trimethylsilanyl-allyl ester methyl ester

Base Information

Chemical Name:Carbonic acid (E)-(R)-1-benzyloxymethyl-3-trimethylsilanyl-allyl ester methyl ester
CAS No.:138722-32-4
Molecular Formula:C₁₆H₂₄O₄Si
Molecular Weight:308.45
Hs Code.:

Synonyms:Carbonic acid (E)-(R)-1-benzyloxymethyl-3-trimethylsilanyl-allyl ester methyl ester

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Chemical Property of Carbonic acid (E)-(R)-1-benzyloxymethyl-3-trimethylsilanyl-allyl ester methyl ester

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Technology Process of Carbonic acid (E)-(R)-1-benzyloxymethyl-3-trimethylsilanyl-allyl ester methyl ester

There total 1 articles about Carbonic acid (E)-(R)-1-benzyloxymethyl-3-trimethylsilanyl-allyl ester methyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 2612-42-2
(dibromomethyl)trimethylsilane

: Carbonic acid (S)-2-benzyloxy-1-formyl-ethyl ester methyl ester

: 138722-32-4
Carbonic acid (E)-(R)-1-benzyloxymethyl-3-trimethylsilanyl-allyl ester methyl ester

Guidance literature:: With chromium dichloride; Yield given;
DOI:10.1021/jo00031a002

Reference yield: 95.0%

: 138722-32-4
Carbonic acid (E)-(R)-1-benzyloxymethyl-3-trimethylsilanyl-allyl ester methyl ester

: 138810-05-6
(E,2R)-1-O-benzyl-4-trimethylsilylbut-3-ene-1,2-diol

Guidance literature:: With lithium aluminium tetrahydride;
DOI:10.1021/jo00031a002

Reference yield:

: 138722-32-4
Carbonic acid (E)-(R)-1-benzyloxymethyl-3-trimethylsilanyl-allyl ester methyl ester

: [(2S,3S)-3-((R)-1-Azido-2-benzyloxy-ethyl)-oxiranyl]-trimethyl-silane

Guidance literature:: Multi-step reaction with 3 steps

1: 95 percent / LiAlH₄

2: 98 percent / Ti(OPrⁱ)4, TBHP, L-(+)-DIPT

3: (PhO)2P(O)N₃, Ph₃P, DEAD

With titanium(IV) isopropylate; tert.-butylhydroperoxide; lithium aluminium tetrahydride; L-(+)-diisopropyl tartrate; diphenyl phosphoryl azide; triphenylphosphine; diethylazodicarboxylate;
DOI:10.1021/jo00031a002