15-benzyloxy-3,7,11,17-tetraaza-bicyclo[11.3.1]heptadeca-1⁽¹⁷⁾,13,15-triene

Base Information

Chemical Name:15-benzyloxy-3,7,11,17-tetraaza-bicyclo[11.3.1]heptadeca-1⁽¹⁷⁾,13,15-triene
CAS No.:1257225-55-0
Molecular Formula:C₂₀H₂₈N₄O
Molecular Weight:340.469
Hs Code.:

15-benzyloxy-3,7,11,17-tetraaza-bicyclo[11.3.1]heptadeca-1<sup>(17)</sup>,13,15-triene

Synonyms:15-benzyloxy-3,7,11,17-tetraaza-bicyclo[11.3.1]heptadeca-1⁽¹⁷⁾,13,15-triene

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Chemical Property of 15-benzyloxy-3,7,11,17-tetraaza-bicyclo[11.3.1]heptadeca-1⁽¹⁷⁾,13,15-triene

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Technology Process of 15-benzyloxy-3,7,11,17-tetraaza-bicyclo[11.3.1]heptadeca-1⁽¹⁷⁾,13,15-triene

There total 1 articles about 15-benzyloxy-3,7,11,17-tetraaza-bicyclo[11.3.1]heptadeca-1⁽¹⁷⁾,13,15-triene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 75.0%

: 56-18-8
bis(3-aminopropyl)amine

: 130567-64-5
4-(benzyloxy)pyridine-2,6-dicarboxaldehyde

: 1257225-55-0
15-benzyloxy-3,7,11,17-tetraaza-bicyclo[11.3.1]heptadeca-1⁽¹⁷⁾,13,15-triene

Guidance literature:: bis(3-aminopropyl)amine; 4-(benzyloxy)pyridine-2,6-dicarboxaldehyde; With copper(II) nitrate trihydrate; In ethanol; water; at 60 ℃; for 6h;

With sodium tetrahydroborate; In methanol; water; at 5 - 60 ℃; Further stages;
DOI:10.1016/j.ica.2010.05.051

Reference yield: 32.0%

: nickel(II) perchlorate hexahydrate

: 1257225-55-0
15-benzyloxy-3,7,11,17-tetraaza-bicyclo[11.3.1]heptadeca-1⁽¹⁷⁾,13,15-triene

: Ni(15-benzyloxy-3,7,11,17-tetraaza-bicyclo[11.3.1]heptadeca-1⁽¹⁷⁾,13,15-triene)(ClO₄)2

Guidance literature:: In methanol; to MeOH soln. of tetraaza-compd. added MeOH soln. of Ni(ClO4)2*6H2O; mixt. heated at 60°C for 30 min; then cooled in ice bath; recrystd. from MeNO2/EtOAc (vapor diffusion method); elem. anal.;
DOI:10.1016/j.ica.2010.05.051