1,2-O-isopropyliden-5-O-allyl-3-O-phenoxycarbonyl-α-D-glucofuranosiduronamide

Base Information

Chemical Name:1,2-O-isopropyliden-5-O-allyl-3-O-phenoxycarbonyl-α-D-glucofuranosiduronamide
CAS No.:220827-22-5
Molecular Formula:C₁₉H₂₃NO₈
Molecular Weight:393.394
Hs Code.:

Synonyms:1,2-O-isopropyliden-5-O-allyl-3-O-phenoxycarbonyl-α-D-glucofuranosiduronamide

Suppliers and Price of 1,2-O-isopropyliden-5-O-allyl-3-O-phenoxycarbonyl-α-D-glucofuranosiduronamide

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Total 1 raw suppliers

Chemical Property of 1,2-O-isopropyliden-5-O-allyl-3-O-phenoxycarbonyl-α-D-glucofuranosiduronamide

Chemical Property:

Purity/Quality:: 98% ^*data from raw suppliers

Safty Information:

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Technology Process of 1,2-O-isopropyliden-5-O-allyl-3-O-phenoxycarbonyl-α-D-glucofuranosiduronamide

There total 3 articles about 1,2-O-isopropyliden-5-O-allyl-3-O-phenoxycarbonyl-α-D-glucofuranosiduronamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 96.0%

: 1885-14-9
phenyl chloroformate

: 156325-49-4
1,2-O-isopropyliden-5-O-allyl-α-D-glucofuranosiduronamide

: 220827-22-5
1,2-O-isopropyliden-5-O-allyl-3-O-phenoxycarbonyl-α-D-glucofuranosiduronamide

Guidance literature:: With dmap; triethylamine; In dichloromethane; at 20 ℃; for 1h;
DOI:10.1016/S0040-4020(98)01063-1

Reference yield:

: 126214-82-2
1,2-O-isopropyliden-5-O-allyl-α-D-glucofuranosidurono-6,3-lactone

: 220827-22-5
1,2-O-isopropyliden-5-O-allyl-3-O-phenoxycarbonyl-α-D-glucofuranosiduronamide

Guidance literature:: Multi-step reaction with 2 steps

1: NH₃ / methanol

2: 96 percent / DMAP / Et₃N / CH₂Cl₂ / 1 h / 20 °C

With dmap; ammonia; triethylamine; In methanol; dichloromethane; 1: Ring cleavage / 2: Esterification;
DOI:10.1016/S0040-4020(98)01063-1

Reference yield:

: 3067-56-9,20513-98-8,25159-39-1,26623-22-3,29514-28-1,85080-95-1
D-glucurono-3,6-lactone acetonide

: 220827-22-5
1,2-O-isopropyliden-5-O-allyl-3-O-phenoxycarbonyl-α-D-glucofuranosiduronamide

Guidance literature:: Multi-step reaction with 3 steps

1: 61 percent / trifluoromethanesulfonic acid

2: NH₃ / methanol

3: 96 percent / DMAP / Et₃N / CH₂Cl₂ / 1 h / 20 °C

With dmap; ammonia; trifluorormethanesulfonic acid; triethylamine; In methanol; dichloromethane; 1: Alkylation / 2: Ring cleavage / 3: Esterification;
DOI:10.1016/S0040-4020(98)01063-1