rac-1-(toluene-4-sulfonyl)-1,2,3,4-tetrahydro-quinoline-4-carboxylic acid methoxy-methyl-amide

Base Information

Chemical Name:rac-1-(toluene-4-sulfonyl)-1,2,3,4-tetrahydro-quinoline-4-carboxylic acid methoxy-methyl-amide
CAS No.:945390-22-7
Molecular Formula:C₁₉H₂₂N₂O₄S
Molecular Weight:374.461
Hs Code.:

Synonyms:rac-1-(toluene-4-sulfonyl)-1,2,3,4-tetrahydro-quinoline-4-carboxylic acid methoxy-methyl-amide

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of rac-1-(toluene-4-sulfonyl)-1,2,3,4-tetrahydro-quinoline-4-carboxylic acid methoxy-methyl-amide

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Technology Process of rac-1-(toluene-4-sulfonyl)-1,2,3,4-tetrahydro-quinoline-4-carboxylic acid methoxy-methyl-amide

There total 1 articles about rac-1-(toluene-4-sulfonyl)-1,2,3,4-tetrahydro-quinoline-4-carboxylic acid methoxy-methyl-amide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 90.0%

: 945390-21-6
rac-1,2,3,4-tetrahydro-quinoline-4-carboxylic acid methoxy-methyl-amide

: 98-59-9
p-toluenesulfonyl chloride

: 945390-22-7
rac-1-(toluene-4-sulfonyl)-1,2,3,4-tetrahydro-quinoline-4-carboxylic acid methoxy-methyl-amide

Guidance literature:: With triethylamine; In 1,2-dichloro-ethane; at 70 ℃; for 4h;

Reference yield: 52.0%

: 945390-22-7
rac-1-(toluene-4-sulfonyl)-1,2,3,4-tetrahydro-quinoline-4-carboxylic acid methoxy-methyl-amide

: 61278-81-7
1-(diethoxymethyl)-1H-imidazole

: 945390-23-8
rac-(1H-imidazol-2-yl)-[1-(toluene-4-sulfonyl)-1,2,3,4-tetrahydro-quinolin-4-yl]-methanone

Guidance literature:: 1-(diethoxymethyl)-1H-imidazole; With n-butyllithium; In tetrahydrofuran; hexane; at -78 ℃;

rac-1-(toluene-4-sulfonyl)-1,2,3,4-tetrahydro-quinoline-4-carboxylic acid methoxy-methyl-amide; In tetrahydrofuran; hexane; at 0 ℃; for 1h;

With hydrogenchloride; water; sodium hydrogencarbonate; more than 3 stages;