(3-Amino-pyrazin-2-yl)-[(S)-2-(tert-butyl-diphenyl-silanyloxymethyl)-pyrrolidin-1-yl]-methanone

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Chemical Name:(3-Amino-pyrazin-2-yl)-[(S)-2-(tert-butyl-diphenyl-silanyloxymethyl)-pyrrolidin-1-yl]-methanone
CAS No.:209627-37-2
Molecular Formula:C₂₆H₃₂N₄O₂Si
Molecular Weight:460.651
Hs Code.:

Synonyms:(3-Amino-pyrazin-2-yl)-[(S)-2-(tert-butyl-diphenyl-silanyloxymethyl)-pyrrolidin-1-yl]-methanone

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Chemical Property of (3-Amino-pyrazin-2-yl)-[(S)-2-(tert-butyl-diphenyl-silanyloxymethyl)-pyrrolidin-1-yl]-methanone

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Technology Process of (3-Amino-pyrazin-2-yl)-[(S)-2-(tert-butyl-diphenyl-silanyloxymethyl)-pyrrolidin-1-yl]-methanone

There total 1 articles about (3-Amino-pyrazin-2-yl)-[(S)-2-(tert-butyl-diphenyl-silanyloxymethyl)-pyrrolidin-1-yl]-methanone which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 100.0%

: 5424-01-1
3-aminopyrazinoic acid

: 209627-36-1
(2S)-2-(((tert-butyldiphenylsilyl)oxy)methyl)idinepyrrol

: 209627-37-2
(3-Amino-pyrazin-2-yl)-[(S)-2-(tert-butyl-diphenyl-silanyloxymethyl)-pyrrolidin-1-yl]-methanone

Guidance literature:: With diethyl cyanophosphonate; triethylamine; In 1,2-dimethoxyethane; 1) 0 deg C, 1 h, 2) room temperature, 1 h;
DOI:10.1016/S0040-4020(98)00256-7

Reference yield:

: 209627-37-2
(3-Amino-pyrazin-2-yl)-[(S)-2-(tert-butyl-diphenyl-silanyloxymethyl)-pyrrolidin-1-yl]-methanone

: 209627-39-4
N-[(2S)-2-(hydroxymethyl)pyrrolidine]-3-(triphenylphosphoranylidene)aminopyrazine-2-carboxamide

Guidance literature:: Multi-step reaction with 2 steps

1: C₂Cl₆, Et₃N / benzene / 2 h / Heating

2: 168 mg / TBAF / tetrahydrofuran / 2 h / Ambient temperature

With hexachloroethane; tetrabutyl ammonium fluoride; triethylamine; In tetrahydrofuran; benzene;
DOI:10.1016/S0040-4020(98)00256-7