3-O,4-S-Dibenzoyl-2,6-dideoxy-4-thio-D-ribo-hexopyranosyl trichloroacetimidate

Base Information

Chemical Name:3-O,4-S-Dibenzoyl-2,6-dideoxy-4-thio-D-ribo-hexopyranosyl trichloroacetimidate
CAS No.:330450-30-1
Molecular Formula:C₂₂H₂₀Cl₃NO₅S
Molecular Weight:516.829
Hs Code.:

Synonyms:3-O,4-S-Dibenzoyl-2,6-dideoxy-4-thio-D-ribo-hexopyranosyl trichloroacetimidate

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Chemical Property of 3-O,4-S-Dibenzoyl-2,6-dideoxy-4-thio-D-ribo-hexopyranosyl trichloroacetimidate

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Technology Process of 3-O,4-S-Dibenzoyl-2,6-dideoxy-4-thio-D-ribo-hexopyranosyl trichloroacetimidate

There total 6 articles about 3-O,4-S-Dibenzoyl-2,6-dideoxy-4-thio-D-ribo-hexopyranosyl trichloroacetimidate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 100.0%

: 545-06-2
trichloroacetonitrile

: 3-O,4-S-Dibenzoyl-2,6-dideoxy-4-thio-D-ribo-hexopyranose

: 330450-30-1
3-O,4-S-Dibenzoyl-2,6-dideoxy-4-thio-D-ribo-hexopyranosyl trichloroacetimidate

Guidance literature:: With 1,8-diazabicyclo[5.4.0]undec-7-ene; In dichloromethane; at 20 ℃; for 1h;
DOI:10.1039/b006113l

Reference yield:

: 126448-25-7
methyl 2,6-dideoxy-4-thio-α-D-ribo-hexopyranoside

: 330450-30-1
3-O,4-S-Dibenzoyl-2,6-dideoxy-4-thio-D-ribo-hexopyranosyl trichloroacetimidate

Guidance literature:: Multi-step reaction with 3 steps

1: 88 percent / pyridine / 5 h / 0 °C / to RT

2: 85 percent / H₂O, AcOH / 2 h / Heating

3: DBU / CH₂Cl₂ / 1 h / Ambient temperature

With pyridine; water; acetic acid; 1,8-diazabicyclo[5.4.0]undec-7-ene; In dichloromethane;
DOI:10.1016/S0040-4039(98)02135-2

Reference yield:

: 98-88-4
benzoyl chloride

: 330450-30-1
3-O,4-S-Dibenzoyl-2,6-dideoxy-4-thio-D-ribo-hexopyranosyl trichloroacetimidate

Guidance literature:: Multi-step reaction with 3 steps

1: 88 percent / pyridine / 5 h / 0 °C / to RT

2: 85 percent / H₂O, AcOH / 2 h / Heating

3: DBU / CH₂Cl₂ / 1 h / Ambient temperature

With pyridine; water; acetic acid; 1,8-diazabicyclo[5.4.0]undec-7-ene; In dichloromethane;
DOI:10.1016/S0040-4039(98)02135-2