(S)-2-phenyl-3-{N-[14-(pyridin-3-yl)tetradec-11-enyl]amino}propanoic acid

Base Information

Chemical Name:(S)-2-phenyl-3-{N-[14-(pyridin-3-yl)tetradec-11-enyl]amino}propanoic acid
CAS No.:1021486-53-2
Molecular Formula:C₂₈H₄₀N₂O₂
Molecular Weight:436.638
Hs Code.:

Synonyms:(S)-2-phenyl-3-{N-[14-(pyridin-3-yl)tetradec-11-enyl]amino}propanoic acid

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Chemical Property of (S)-2-phenyl-3-{N-[14-(pyridin-3-yl)tetradec-11-enyl]amino}propanoic acid

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Technology Process of (S)-2-phenyl-3-{N-[14-(pyridin-3-yl)tetradec-11-enyl]amino}propanoic acid

There total 15 articles about (S)-2-phenyl-3-{N-[14-(pyridin-3-yl)tetradec-11-enyl]amino}propanoic acid which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: C₄₁H₆₁N₃O₅

: 1021486-53-2
(S)-2-phenyl-3-{N-[14-(pyridin-3-yl)tetradec-11-enyl]amino}propanoic acid

: 223906-38-5
(4R)-5,5-dimethyl-4-(propan-2-yl)-1,3-oxazolidin-2-one

Guidance literature:: C₄₁H₆₁N₃O₅; With dihydrogen peroxide; lithium hydroxide; In tetrahydrofuran; water; at 0 - 20 ℃; for 16h;

With hydrogenchloride; In diethyl ether; at 20 ℃; for 0.5h;
DOI:10.1016/j.tetlet.2013.09.043

Reference yield:

: 73010-80-7
1-tetrahydropyranyloxyundecyl-11-triphenylphosphonium bromide

: 1021486-53-2
(S)-2-phenyl-3-{N-[14-(pyridin-3-yl)tetradec-11-enyl]amino}propanoic acid

Guidance literature:: Multi-step reaction with 7 steps

1.1: potassium hexamethylsilazane / tetrahydrofuran; toluene / 1 h / -78 - 20 °C / Inert atmosphere

1.2: 2.08 h / -78 - 20 °C / Inert atmosphere

2.1: hydrogenchloride / methanol; water / 16 h / 20 °C

3.1: 1-hydroxy-3H-benz[d][1,2]iodoxole-1,3-dione / ethyl acetate / 3 h / 20 - 80 °C / Inert atmosphere

4.1: sodium tris(acetoxy)borohydride; acetic acid / 1,2-dichloro-ethane / 16 h / 20 °C / Inert atmosphere

5.1: ammonium cerium (IV) nitrate / acetonitrile; water / 16 h / 20 °C

6.1: sodium hydrogencarbonate / ethanol / 16 h / 0 - 20 °C / Inert atmosphere

7.1: lithium hydroxide; dihydrogen peroxide / tetrahydrofuran; water / 16 h / 0 - 20 °C

7.2: 0.5 h / 20 °C

With hydrogenchloride; ammonium cerium (IV) nitrate; dihydrogen peroxide; potassium hexamethylsilazane; sodium tris(acetoxy)borohydride; sodium hydrogencarbonate; acetic acid; lithium hydroxide; 1-hydroxy-3H-benz[d][1,2]iodoxole-1,3-dione; In tetrahydrofuran; methanol; ethanol; water; ethyl acetate; 1,2-dichloro-ethane; toluene; acetonitrile;
DOI:10.1016/j.tetlet.2013.09.043

Reference yield:

: 2859-67-8
3-(3-pyridyl)propan-1-ol

: 1021486-53-2
(S)-2-phenyl-3-{N-[14-(pyridin-3-yl)tetradec-11-enyl]amino}propanoic acid

Guidance literature:: Multi-step reaction with 8 steps

1.1: oxalyl dichloride; dimethyl sulfoxide / dichloromethane / 0.67 h / -78 °C / Inert atmosphere

1.2: 1.5 h / 20 °C / Inert atmosphere

2.1: potassium hexamethylsilazane / tetrahydrofuran; toluene / 1 h / -78 - 20 °C / Inert atmosphere

2.2: 2.08 h / -78 - 20 °C / Inert atmosphere

3.1: hydrogenchloride / methanol; water / 16 h / 20 °C

4.1: 1-hydroxy-3H-benz[d][1,2]iodoxole-1,3-dione / ethyl acetate / 3 h / 20 - 80 °C / Inert atmosphere

5.1: sodium tris(acetoxy)borohydride; acetic acid / 1,2-dichloro-ethane / 16 h / 20 °C / Inert atmosphere

6.1: ammonium cerium (IV) nitrate / acetonitrile; water / 16 h / 20 °C

7.1: sodium hydrogencarbonate / ethanol / 16 h / 0 - 20 °C / Inert atmosphere

8.1: lithium hydroxide; dihydrogen peroxide / tetrahydrofuran; water / 16 h / 0 - 20 °C

8.2: 0.5 h / 20 °C

With hydrogenchloride; ammonium cerium (IV) nitrate; oxalyl dichloride; dihydrogen peroxide; potassium hexamethylsilazane; sodium tris(acetoxy)borohydride; sodium hydrogencarbonate; acetic acid; dimethyl sulfoxide; lithium hydroxide; 1-hydroxy-3H-benz[d][1,2]iodoxole-1,3-dione; In tetrahydrofuran; methanol; ethanol; dichloromethane; water; ethyl acetate; 1,2-dichloro-ethane; toluene; acetonitrile; 1.1: |Swern Oxidation / 1.2: |Swern Oxidation;
DOI:10.1016/j.tetlet.2013.09.043