C₂₀H₃₃NO₃Si

Base Information

Chemical Name:C₂₀H₃₃NO₃Si
CAS No.:1332652-84-2
Molecular Formula:C₂₀H₃₃NO₃Si
Molecular Weight:363.572
Hs Code.:

C<sub>20</sub>H<sub>33</sub>NO<sub>3</sub>Si

Synonyms:C₂₀H₃₃NO₃Si

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Chemical Property of C₂₀H₃₃NO₃Si

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Technology Process of C₂₀H₃₃NO₃Si

There total 4 articles about C₂₀H₃₃NO₃Si which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1332652-82-0
(2R)-2-benzyloxy-4-hydroxy-N-methoxy-N,3,3-trimethylbutanamide

: 1332652-84-2
C₂₀H₃₃NO₃Si

Guidance literature:: Multi-step reaction with 3 steps

1.1: oxalyl dichloride; dimethyl sulfoxide / 0.83 h / -78 °C

1.2: 16 h / -78 - 20 °C

2.1: sodium tris(acetoxy)borohydride; acetic acid; triethylamine / dichloromethane / 1 h / 20 °C

3.1: palladium on activated charcoal; hydrogen

With oxalyl dichloride; palladium on activated charcoal; hydrogen; sodium tris(acetoxy)borohydride; acetic acid; dimethyl sulfoxide; triethylamine; In dichloromethane; 1.1: Swern oxidation / 1.2: Swern oxidation;
DOI:10.1016/j.tetlet.2011.07.021

Reference yield:

: 1351413-93-8
C₁₅H₂₁NO₄

: 1332652-84-2
C₂₀H₃₃NO₃Si

Guidance literature:: Multi-step reaction with 2 steps

1: sodium tris(acetoxy)borohydride; acetic acid; triethylamine / dichloromethane / 1 h / 20 °C

2: palladium on activated charcoal; hydrogen

With palladium on activated charcoal; hydrogen; sodium tris(acetoxy)borohydride; acetic acid; triethylamine; In dichloromethane;
DOI:10.1016/j.tetlet.2011.07.021

Reference yield:

: 20374-33-8
(R)-(+)-3-(Benzyloxy)-4,5-dihydro-4,4-dimethyl-furan-2(3H)-on

: 1332652-84-2
C₂₀H₃₃NO₃Si

Guidance literature:: Multi-step reaction with 4 steps

1.1: isopropylmagnesium chloride / tetrahydrofuran / 0 °C

1.2: 0 °C / pH 7 / aq. phosphate buffer

2.1: oxalyl dichloride; dimethyl sulfoxide / 0.83 h / -78 °C

2.2: 16 h / -78 - 20 °C

3.1: sodium tris(acetoxy)borohydride; acetic acid; triethylamine / dichloromethane / 1 h / 20 °C

4.1: palladium on activated charcoal; hydrogen

With oxalyl dichloride; palladium on activated charcoal; hydrogen; isopropylmagnesium chloride; sodium tris(acetoxy)borohydride; acetic acid; dimethyl sulfoxide; triethylamine; In tetrahydrofuran; dichloromethane; 2.1: Swern oxidation / 2.2: Swern oxidation;
DOI:10.1016/j.tetlet.2011.07.021