[2,6-dichloro-4-(3,6-dimethoxy-N-carbazolyl)phenyl]bis(2,4,6-trichlorophenyl)methane

Base Information

Chemical Name:[2,6-dichloro-4-(3,6-dimethoxy-N-carbazolyl)phenyl]bis(2,4,6-trichlorophenyl)methane
CAS No.:955094-67-4
Molecular Formula:C₃₃H₁₉Cl₈NO₂
Molecular Weight:745.143
Hs Code.:

Synonyms:[2,6-dichloro-4-(3,6-dimethoxy-N-carbazolyl)phenyl]bis(2,4,6-trichlorophenyl)methane

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Chemical Property of [2,6-dichloro-4-(3,6-dimethoxy-N-carbazolyl)phenyl]bis(2,4,6-trichlorophenyl)methane

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Technology Process of [2,6-dichloro-4-(3,6-dimethoxy-N-carbazolyl)phenyl]bis(2,4,6-trichlorophenyl)methane

There total 1 articles about [2,6-dichloro-4-(3,6-dimethoxy-N-carbazolyl)phenyl]bis(2,4,6-trichlorophenyl)methane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 44.0%

: 109745-46-2
tris(2,4,6‐trichlorophenyl)methyl radical

: 57103-01-2
3,6-di-methoxy-9H-carbazole

: 955094-67-4
[2,6-dichloro-4-(3,6-dimethoxy-N-carbazolyl)phenyl]bis(2,4,6-trichlorophenyl)methane

: 105633-27-0
tris(2,4,6-trichlorophenyl)methane

Guidance literature:: With caesium carbonate; In N,N-dimethyl-formamide; for 2.5h; Heating;
DOI:10.1021/jo0708846

Reference yield: 85.0%

: 955094-67-4
[2,6-dichloro-4-(3,6-dimethoxy-N-carbazolyl)phenyl]bis(2,4,6-trichlorophenyl)methane

: 955094-73-2
[2,6-dichloro-4-(3,6-dimethoxy-N-carbazolyl)phenyl]bis(2,4,6-trichlorophenyl)methyl

Guidance literature:: [2,6-dichloro-4-(3,6-dimethoxy-N-carbazolyl)phenyl]bis(2,4,6-trichlorophenyl)methane; With sodium hydroxide; In diethyl ether; dimethyl sulfoxide; at 20 ℃; for 48h;

With iodine; In diethyl ether; dimethyl sulfoxide; for 1h; Further stages.;
DOI:10.1021/jo0708846

Reference yield:

: 955094-67-4
[2,6-dichloro-4-(3,6-dimethoxy-N-carbazolyl)phenyl]bis(2,4,6-trichlorophenyl)methane

: C₃₃H₁₈Cl₈NO₂^(1-)*C₁₆H₃₆N⁽¹⁺⁾

Guidance literature:: Multi-step reaction with 2 steps

1.1: sodium hydroxide / diethyl ether; dimethylsulfoxide / 48 h / 20 °C

1.2: 85 percent / iodine / diethyl ether; dimethylsulfoxide / 1 h

2.1: H₂O; tetrahydrofuran

With sodium hydroxide; In tetrahydrofuran; diethyl ether; water; dimethyl sulfoxide;
DOI:10.1021/jo0708846