1,6-bis(3,3,3-triphenylprop-1-ynyl)perylene-3,4:9,10-tetracarboxylic acid anhydride

Base Information

Chemical Name:1,6-bis(3,3,3-triphenylprop-1-ynyl)perylene-3,4:9,10-tetracarboxylic acid anhydride
CAS No.:1325731-52-9
Molecular Formula:C₆₆H₃₆O₆
Molecular Weight:925.008
Hs Code.:

Synonyms:1,6-bis(3,3,3-triphenylprop-1-ynyl)perylene-3,4:9,10-tetracarboxylic acid anhydride

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Chemical Property of 1,6-bis(3,3,3-triphenylprop-1-ynyl)perylene-3,4:9,10-tetracarboxylic acid anhydride

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Technology Process of 1,6-bis(3,3,3-triphenylprop-1-ynyl)perylene-3,4:9,10-tetracarboxylic acid anhydride

There total 3 articles about 1,6-bis(3,3,3-triphenylprop-1-ynyl)perylene-3,4:9,10-tetracarboxylic acid anhydride which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 75.0%

: 1325731-46-1
1,6-bis((3,3,3-triphenylprop-1-ynyl))-N,N'-bis(1-ethylpropyl)perylene-3,4:9,10-tetracarboxylic acid bisimide

: 1325731-52-9
1,6-bis(3,3,3-triphenylprop-1-ynyl)perylene-3,4:9,10-tetracarboxylic acid anhydride

Guidance literature:: 1,6-bis((3,3,3-triphenylprop-1-ynyl))-N,N'-bis(1-ethylpropyl)perylene-3,4:9,10-tetracarboxylic acid bisimide; With potassium hydroxide; In tert-butyl alcohol; Reflux;

With acetic acid; at 50 ℃; for 0.5h;
DOI:10.1021/ol2019407

Reference yield:

: 110590-81-3
N,N'-bis(1-ethylpropyl)-3,4:9,10-perylenebis(dicarboximide)

: 1325731-52-9
1,6-bis(3,3,3-triphenylprop-1-ynyl)perylene-3,4:9,10-tetracarboxylic acid anhydride

Guidance literature:: Multi-step reaction with 2 steps

1.1: bromine / dichloromethane / 86 h / 50 °C

1.2: 24 h / 90 °C / Inert atmosphere

2.1: potassium hydroxide / tert-butyl alcohol / Reflux

2.2: 0.5 h / 50 °C

With bromine; potassium hydroxide; In dichloromethane; tert-butyl alcohol; 1.2: Sonogashira cross-coupling;
DOI:10.1021/ol2019407

Reference yield:

: 128-69-8
perylene-3,4,9,10-tetracarboxylic acid 3,4:9,10-dianhydride

: 1325731-52-9
1,6-bis(3,3,3-triphenylprop-1-ynyl)perylene-3,4:9,10-tetracarboxylic acid anhydride

Guidance literature:: Multi-step reaction with 3 steps

1.1: 1H-imidazole / 4 h / 140 °C

2.1: bromine / dichloromethane / 86 h / 50 °C

2.2: 24 h / 90 °C / Inert atmosphere

3.1: potassium hydroxide / tert-butyl alcohol / Reflux

3.2: 0.5 h / 50 °C

With 1H-imidazole; bromine; potassium hydroxide; In dichloromethane; tert-butyl alcohol; 2.2: Sonogashira cross-coupling;
DOI:10.1021/ol2019407