C₇₉H₁₂₈O₁₃Si₃

Base Information

Chemical Name:C₇₉H₁₂₈O₁₃Si₃
CAS No.:863663-09-6
Molecular Formula:C₇₉H₁₂₈O₁₃Si₃
Molecular Weight:1370.13
Hs Code.:

C<sub>79</sub>H<sub>128</sub>O<sub>13</sub>Si<sub>3</sub>

Synonyms:C₇₉H₁₂₈O₁₃Si₃

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Chemical Property of C₇₉H₁₂₈O₁₃Si₃

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Technology Process of C₇₉H₁₂₈O₁₃Si₃

There total 30 articles about C₇₉H₁₂₈O₁₃Si₃ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 863660-01-9
((2R,6S)-6-Benzyloxymethyl-tetrahydro-pyran-2-yl)-acetaldehyde

: 863663-09-6
C₇₉H₁₂₈O₁₃Si₃

Guidance literature:: Multi-step reaction with 8 steps

1.1: hexamethylphosphoric acid triamide; tetrahydrofuran / -30 °C

2.1: n-BuLi / tetrahydrofuran / -78 °C

3.1: n-Bu₃SnH; AIBN / benzene / Heating

3.2: PdCl₂(PPh₃)2; LiCl; Ph₃P / dimethylformamide / 120 °C

4.1: H₂ / Pd/C / methanol

5.1: SO₃*Py; TEA / dimethylsulfoxide; CH₂Cl₂ / 0 °C

6.1: NaHMDS / tetrahydrofuran; diethyl ether / 0.25 h / -78 °C

6.2: 83 percent / tetrahydrofuran; diethyl ether / 10 h / -78 - 20 °C

7.1: TsNHNH₂; aq. NaOAc / 1,2-dimethoxy-ethane / Heating

8.1: NaHMDS / tetrahydrofuran / 0 °C

8.2: tetrahydrofuran

With n-butyllithium; pyridine-SO₃ complex; 2,2'-azobis(isobutyronitrile); TEA; hydrogen; tri-n-butyl-tin hydride; sodium acetate; sodium hexamethyldisilazane; toluene-4-sulfonic acid hydrazide; palladium on activated charcoal; In tetrahydrofuran; methanol; N,N,N,N,N,N-hexamethylphosphoric triamide; 1,2-dimethoxyethane; diethyl ether; dichloromethane; dimethyl sulfoxide; benzene; 3.2: Stille coupling / 6.2: Julia-Julia olefination;
DOI:10.1021/ja0315309

Reference yield:

: 863662-92-4
(-)-2-((2R,6S)-6-((benzyloxy)methyl)tetrahydro-2H-pyran-2-yl)ethanol

: 863663-09-6
C₇₉H₁₂₈O₁₃Si₃

Guidance literature:: Multi-step reaction with 9 steps

1.1: SO₃*Py; TEA / dimethylsulfoxide; CH₂Cl₂ / 0 °C

2.1: hexamethylphosphoric acid triamide; tetrahydrofuran / -30 °C

3.1: n-BuLi / tetrahydrofuran / -78 °C

4.1: n-Bu₃SnH; AIBN / benzene / Heating

4.2: PdCl₂(PPh₃)2; LiCl; Ph₃P / dimethylformamide / 120 °C

5.1: H₂ / Pd/C / methanol

6.1: SO₃*Py; TEA / dimethylsulfoxide; CH₂Cl₂ / 0 °C

7.1: NaHMDS / tetrahydrofuran; diethyl ether / 0.25 h / -78 °C

7.2: 83 percent / tetrahydrofuran; diethyl ether / 10 h / -78 - 20 °C

8.1: TsNHNH₂; aq. NaOAc / 1,2-dimethoxy-ethane / Heating

9.1: NaHMDS / tetrahydrofuran / 0 °C

9.2: tetrahydrofuran

With n-butyllithium; pyridine-SO₃ complex; 2,2'-azobis(isobutyronitrile); TEA; hydrogen; tri-n-butyl-tin hydride; sodium acetate; sodium hexamethyldisilazane; toluene-4-sulfonic acid hydrazide; palladium on activated charcoal; In tetrahydrofuran; methanol; N,N,N,N,N,N-hexamethylphosphoric triamide; 1,2-dimethoxyethane; diethyl ether; dichloromethane; dimethyl sulfoxide; benzene; 4.2: Stille coupling / 7.2: Julia-Julia olefination;
DOI:10.1021/ja0315309

Reference yield:

: 863662-94-6
(2S,6R)-2-Benzyloxymethyl-6-prop-2-ynyl-tetrahydro-pyran

: 863663-09-6
C₇₉H₁₂₈O₁₃Si₃

Guidance literature:: Multi-step reaction with 6 steps

1.1: n-Bu₃SnH; AIBN / benzene / Heating

1.2: PdCl₂(PPh₃)2; LiCl; Ph₃P / dimethylformamide / 120 °C

2.1: H₂ / Pd/C / methanol

3.1: SO₃*Py; TEA / dimethylsulfoxide; CH₂Cl₂ / 0 °C

4.1: NaHMDS / tetrahydrofuran; diethyl ether / 0.25 h / -78 °C

4.2: 83 percent / tetrahydrofuran; diethyl ether / 10 h / -78 - 20 °C

5.1: TsNHNH₂; aq. NaOAc / 1,2-dimethoxy-ethane / Heating

6.1: NaHMDS / tetrahydrofuran / 0 °C

6.2: tetrahydrofuran

With pyridine-SO₃ complex; 2,2'-azobis(isobutyronitrile); TEA; hydrogen; tri-n-butyl-tin hydride; sodium acetate; sodium hexamethyldisilazane; toluene-4-sulfonic acid hydrazide; palladium on activated charcoal; In tetrahydrofuran; methanol; 1,2-dimethoxyethane; diethyl ether; dichloromethane; dimethyl sulfoxide; benzene; 1.2: Stille coupling / 4.2: Julia-Julia olefination;
DOI:10.1021/ja0315309