11,17-Dichlor-29-dioctylamino-14-(p-tolyl)-2,8,10,12,14,16,18,20,26,28,30,31,33,34-tetradecaazahexacyclo[25.3.1.1^3,7.1^9,13.1^15,19.1^21,25]pentatriaconta-1⁽³¹⁾,3,5,7⁽³⁵⁾,9,11,13⁽³⁴⁾,15,17,19⁽³³⁾,21,23,25⁽³²⁾,27,29-pentadecaene

Base Information

• Chemical Name: 11,17-Dichlor-29-dioctylamino-14-(p-tolyl)-2,8,10,12,14,16,18,20,26,28,30,31,33,34-tetradecaazahexacyclo[25.3.1.1^3,7.1^9,13.1^15,19.1^21,25]pentatriaconta-1⁽³¹⁾,3,5,7⁽³⁵⁾,9,11,13⁽³⁴⁾,15,17,19⁽³³⁾,21,23,25⁽³²⁾,27,29-pentadecaene
• CAS No.: 190138-15-9
• Molecular Formula: C₄₄H₅₃Cl₂N₁₅
• Molecular Weight: 862.911

Synonyms:11,17-Dichlor-29-dioctylamino-14-(p-tolyl)-2,8,10,12,14,16,18,20,26,28,30,31,33,34-tetradecaazahexacyclo[25.3.1.1^3,7.1^9,13.1^15,19.1^21,25]pentatriaconta-1⁽³¹⁾,3,5,7⁽³⁵⁾,9,11,13⁽³⁴⁾,15,17,19⁽³³⁾,21,23,25⁽³²⁾,27,29-pentadecaene

Chemical Property of 11,17-Dichlor-29-dioctylamino-14-(p-tolyl)-2,8,10,12,14,16,18,20,26,28,30,31,33,34-tetradecaazahexacyclo[25.3.1.1^3,7.1^9,13.1^15,19.1^21,25]pentatriaconta-1⁽³¹⁾,3,5,7⁽³⁵⁾,9,11,13⁽³⁴⁾,15,17,19⁽³³⁾,21,23,25⁽³²⁾,27,29-pentadecaene

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Technology Process of 11,17-Dichlor-29-dioctylamino-14-(p-tolyl)-2,8,10,12,14,16,18,20,26,28,30,31,33,34-tetradecaazahexacyclo[25.3.1.1^3,7.1^9,13.1^15,19.1^21,25]pentatriaconta-1⁽³¹⁾,3,5,7⁽³⁵⁾,9,11,13⁽³⁴⁾,15,17,19⁽³³⁾,21,23,25⁽³²⁾,27,29-pentadecaene

There total 3 articles about 11,17-Dichlor-29-dioctylamino-14-(p-tolyl)-2,8,10,12,14,16,18,20,26,28,30,31,33,34-tetradecaazahexacyclo[25.3.1.1^3,7.1^9,13.1^15,19.1^21,25]pentatriaconta-1⁽³¹⁾,3,5,7⁽³⁵⁾,9,11,13⁽³⁴⁾,15,17,19⁽³³⁾,21,23,25⁽³²⁾,27,29-pentadecaene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 43.0%

bis-(4,6-dichloro-[1,3,5]triazin-2-yl)-p-tolyl-amine (27315-13-5) + N,N'-Bis-(3-amino-phenyl)-N'',N''-dioctyl-[1,3,5]triazine-2,4,6-triamine (190138-06-8) → 11,17-Dichlor-29-dioctylamino-14-(p-tolyl)-2,8,10,12,14,16,18,20,26,28,30,31,33,34-tetradecaazahexacyclo[25.3.1.13,7.19,13.115,19.121,25]pentatriaconta-1(31),3,5,7(35),9,11,13(34),15,17,19(33),21,23,25(32),27,29-pentadecaene (190138-15-9)

Guidance literature:

With potassium carbonate; In acetone; at 25 ℃; for 1.5h;

DOI:10.1002/prac.19973390147

Reference yield:

n-dioctylamine (1120-48-5) → 11,17-Dichlor-29-dioctylamino-14-(p-tolyl)-2,8,10,12,14,16,18,20,26,28,30,31,33,34-tetradecaazahexacyclo[25.3.1.13,7.19,13.115,19.121,25]pentatriaconta-1(31),3,5,7(35),9,11,13(34),15,17,19(33),21,23,25(32),27,29-pentadecaene (190138-15-9)

Guidance literature:

Multi-step reaction with 3 steps

1: 22 percent / K₂CO₃ / acetone / 0.5 h / 0 °C

2: 74 percent / Na₂CO₃ / dioxane / 5 h / Heating

3: 43 percent / K₂CO₃ / acetone / 1.5 h / 25 °C

With sodium carbonate; potassium carbonate; In 1,4-dioxane; acetone;

DOI:10.1002/prac.19973390147

Reference yield:

6-N,N-dioctylamiono-1,3,5-triazine-2,4-dichloride (117047-57-1) → 11,17-Dichlor-29-dioctylamino-14-(p-tolyl)-2,8,10,12,14,16,18,20,26,28,30,31,33,34-tetradecaazahexacyclo[25.3.1.13,7.19,13.115,19.121,25]pentatriaconta-1(31),3,5,7(35),9,11,13(34),15,17,19(33),21,23,25(32),27,29-pentadecaene (190138-15-9)

Guidance literature:

Multi-step reaction with 2 steps

1: 74 percent / Na₂CO₃ / dioxane / 5 h / Heating

2: 43 percent / K₂CO₃ / acetone / 1.5 h / 25 °C

With sodium carbonate; potassium carbonate; In 1,4-dioxane; acetone;

DOI:10.1002/prac.19973390147

upstream raw materials:

bis-(4,6-dichloro-[1,3,5]triazin-2-yl)-p-tolyl-amine

N,N'-Bis-(3-amino-phenyl)-N'',N''-dioctyl-[1,3,5]triazine-2,4,6-triamine

n-dioctylamine

6-N,N-dioctylamiono-1,3,5-triazine-2,4-dichloride

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