N^2'-acetyl-7-L-<<<4-<<<1,3-bis(tert-butoxycarbonyl)-propyl>amino>carbonyl>phenyl>imino>methyl>pterin

Base Information

• Chemical Name: N^2'-acetyl-7-L-<<<4-<<<1,3-bis(tert-butoxycarbonyl)-propyl>amino>carbonyl>phenyl>imino>methyl>pterin
• CAS No.: 76282-71-8
• Molecular Formula: C₂₉H₃₅N₇O₇
• Molecular Weight: 593.64

Synonyms:N^2'-acetyl-7-L-<<<4-<<<1,3-bis(tert-butoxycarbonyl)-propyl>amino>carbonyl>phenyl>imino>methyl>pterin

Chemical Property of N^2'-acetyl-7-L-<<<4-<<<1,3-bis(tert-butoxycarbonyl)-propyl>amino>carbonyl>phenyl>imino>methyl>pterin

Chemical Property:

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Technology Process of N^2'-acetyl-7-L-<<<4-<<<1,3-bis(tert-butoxycarbonyl)-propyl>amino>carbonyl>phenyl>imino>methyl>pterin

There total 4 articles about N^2'-acetyl-7-L-<<<4-<<<1,3-bis(tert-butoxycarbonyl)-propyl>amino>carbonyl>phenyl>imino>methyl>pterin which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 76.0%

di-tert-butyl (S)-N-(p-aminobenzoyl)-glutamate (76282-66-1) + N2'-acetyl-7-formylpterin (76282-69-4) → N2'-acetyl-7-L-<<<4-<<<1,3-bis(tert-butoxycarbonyl)-propyl>amino>carbonyl>phenyl>imino>methyl>pterin (76282-71-8)

Guidance literature:

In ethanol; for 2h; Heating;

DOI:10.1021/jo00320a034

Reference yield:

7-formylpterin dimethyl acetal (76299-38-2) → N2'-acetyl-7-L-<<<4-<<<1,3-bis(tert-butoxycarbonyl)-propyl>amino>carbonyl>phenyl>imino>methyl>pterin (76282-71-8)

Guidance literature:

Multi-step reaction with 3 steps

1: 100 percent / 1 N HCl / H₂O / 110 °C

2: 88 percent / 0.5 h / Heating

3: 76 percent / ethanol / 2 h / Heating

With hydrogenchloride; In ethanol; water;

DOI:10.1021/jo00320a034

Reference yield:

2,4-diamino-7-formyl-pteridine dimethyl acetal (76299-37-1) → N2'-acetyl-7-L-<<<4-<<<1,3-bis(tert-butoxycarbonyl)-propyl>amino>carbonyl>phenyl>imino>methyl>pterin (76282-71-8)

Guidance literature:

Multi-step reaction with 4 steps

1: 90 percent / 5percent NaOH / H₂O / 0.08 h / Heating

2: 100 percent / 1 N HCl / H₂O / 110 °C

3: 88 percent / 0.5 h / Heating

4: 76 percent / ethanol / 2 h / Heating

With hydrogenchloride; sodium hydroxide; In ethanol; water;

DOI:10.1021/jo00320a034

upstream raw materials:

di-tert-butyl (S)-N-(p-aminobenzoyl)-glutamate

N^2'-acetyl-7-formylpterin

7-formylpterin

7-formylpterin dimethyl acetal

Downstream raw materials:

N^2'-acetyl-7-L-<<<4-<<<1,3-bis(tert-butoxycarbonyl)-propyl>amino>carbonyl>phenyl>amino>methyl>pterin

N^2'-acetyl-7-folic acid

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