Technology Process of C29H19F5N2O2
There total 2 articles about C29H19F5N2O2 which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
2-(2-methoxyphenyl)pyrrole; perfluorobenzaldehyde;
With
trifluoroacetic acid;
In
dichloromethane;
at 20 ℃;
for 1h;
Inert atmosphere;
Schlenk technique;
With
chloranil;
In
dichloromethane;
at 20 ℃;
for 1h;
Inert atmosphere;
Schlenk technique;
DOI:10.1002/ejoc.201402446
- Guidance literature:
-
Multi-step reaction with 2 steps
1.1: sodium hydride; zinc(II) chloride / mineral oil; tetrahydrofuran / 0.5 h / Schlenk technique; Inert atmosphere
1.2: 24 h / 65 °C / Schlenk technique; Inert atmosphere; Reflux
2.1: trifluoroacetic acid / dichloromethane / 1 h / 20 °C / Inert atmosphere; Schlenk technique
2.2: 1 h / 20 °C / Inert atmosphere; Schlenk technique
With
sodium hydride; trifluoroacetic acid; zinc(II) chloride;
In
tetrahydrofuran; dichloromethane; mineral oil;
DOI:10.1002/ejoc.201402446
- Guidance literature:
-
Multi-step reaction with 2 steps
1.1: boron tribromide / dichloromethane / 12 h / 0 - 20 °C / Inert atmosphere; Schlenk technique
1.2: 3 h / Inert atmosphere; Schlenk technique; Reflux
2.1: tetrabutyl-ammonium chloride / [(2)H6]acetone
With
tetrabutyl-ammonium chloride; boron tribromide;
In
[(2)H6]acetone; dichloromethane;
DOI:10.1002/ejoc.201402446