N-(6-(4-(5-amino-1,3,4-thiadiazol-2-yl)butyl)pyridazin-3-yl)-2-phenylethanamide

Base Information

Chemical Name:N-(6-(4-(5-amino-1,3,4-thiadiazol-2-yl)butyl)pyridazin-3-yl)-2-phenylethanamide
CAS No.:1439394-33-8
Molecular Formula:C₁₈H₂₀N₆OS
Molecular Weight:368.462
Hs Code.:

Synonyms:N-(6-(4-(5-amino-1,3,4-thiadiazol-2-yl)butyl)pyridazin-3-yl)-2-phenylethanamide

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Chemical Property of N-(6-(4-(5-amino-1,3,4-thiadiazol-2-yl)butyl)pyridazin-3-yl)-2-phenylethanamide

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Technology Process of N-(6-(4-(5-amino-1,3,4-thiadiazol-2-yl)butyl)pyridazin-3-yl)-2-phenylethanamide

There total 6 articles about N-(6-(4-(5-amino-1,3,4-thiadiazol-2-yl)butyl)pyridazin-3-yl)-2-phenylethanamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1439400-09-5
N-(6-(4-cyanobutyl)pyridazin-3-yl)-2-phenylacetamide

: 79-19-6
thiosemicarbazide

: 1439394-33-8
N-(6-(4-(5-amino-1,3,4-thiadiazol-2-yl)butyl)pyridazin-3-yl)-2-phenylethanamide

Guidance literature:: With trifluoroacetic acid; at 65 ℃; for 2h; Concentration; Temperature; Time;

Reference yield:

: 103-80-0
phenylacetyl chloride

: 1439394-33-8
N-(6-(4-(5-amino-1,3,4-thiadiazol-2-yl)butyl)pyridazin-3-yl)-2-phenylethanamide

Guidance literature:: Multi-step reaction with 3 steps

1: 1-methyl-pyrrolidin-2-one / 1.58 h / 19 - 28 °C

2: 1,3-bis[(diphenylphosphino)propane]dichloronickel(II) / tetrahydrofuran / 4 h / 19 °C / Inert atmosphere

3: trifluoroacetic acid / 2 h / 65 °C

With 1,3-bis[(diphenylphosphino)propane]dichloronickel(II); trifluoroacetic acid; In tetrahydrofuran; 1-methyl-pyrrolidin-2-one;

Reference yield:

: 19596-07-7
pent-4-ynenitrile

: 1439394-33-8
N-(6-(4-(5-amino-1,3,4-thiadiazol-2-yl)butyl)pyridazin-3-yl)-2-phenylethanamide

Guidance literature:: Multi-step reaction with 3 steps

1: bis-triphenylphosphine-palladium(II) chloride; copper(l) iodide; triethylamine / tetrahydrofuran / 60 °C / Inert atmosphere

2: hydrogen; 10 wt% Pd(OH)2 on carbon / ethanol; ethyl acetate / 1 h

3: trifluoroacetic acid / 2 h / 65 °C

With bis-triphenylphosphine-palladium(II) chloride; copper(l) iodide; 10 wt% Pd(OH)2 on carbon; hydrogen; triethylamine; trifluoroacetic acid; In tetrahydrofuran; ethanol; ethyl acetate;