(2R,3S)-3-O-benzyl-1,2-O-isopropylidene-4-<2-(5-methylfuryl)>-1,2,3-butanetriol

Base Information

Chemical Name:(2R,3S)-3-O-benzyl-1,2-O-isopropylidene-4-<2-(5-methylfuryl)>-1,2,3-butanetriol
CAS No.:93170-24-2
Molecular Formula:C₁₉H₂₄O₄
Molecular Weight:316.397
Hs Code.:

Synonyms:(2R,3S)-3-O-benzyl-1,2-O-isopropylidene-4-<2-(5-methylfuryl)>-1,2,3-butanetriol

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Chemical Property of (2R,3S)-3-O-benzyl-1,2-O-isopropylidene-4-<2-(5-methylfuryl)>-1,2,3-butanetriol

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Technology Process of (2R,3S)-3-O-benzyl-1,2-O-isopropylidene-4-<2-(5-methylfuryl)>-1,2,3-butanetriol

There total 3 articles about (2R,3S)-3-O-benzyl-1,2-O-isopropylidene-4-<2-(5-methylfuryl)>-1,2,3-butanetriol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 625-86-5
2,5-dimethylfuran

: 93170-24-2
(2R,3S)-3-O-benzyl-1,2-O-isopropylidene-4-<2-(5-methylfuryl)>-1,2,3-butanetriol

Guidance literature:: Multi-step reaction with 2 steps

1: 22 percent / CH₂Cl₂ / 24 h / 50 °C / 15001200 Torr

2: 1.) NaH / 1.) THHF, DMF, rt., 0.5 h, 2.) THF, DMF, 12 h

With sodium hydride; In dichloromethane;
DOI:10.1016/S0040-4020(01)86159-7

Reference yield:

: 100-39-0
benzyl bromide

: 89215-49-6
1-(2,2-Dimethyl-[1,3]dioxolan-4-yl)-2-(5-methyl-furan-2-yl)-ethanol

: 93170-25-3
(2R,3R)-3-O-benzyl-1,2-O-isopropylidene-4-<2-(5-methylfuryl)>-1,2,3-butanetriol

: 93170-24-2
(2R,3S)-3-O-benzyl-1,2-O-isopropylidene-4-<2-(5-methylfuryl)>-1,2,3-butanetriol

Guidance literature:: With sodium hydride; In tetrahydrofuran; N,N-dimethyl-formamide; Ambient temperature;
DOI:10.1016/0040-4039(84)80020-9

Reference yield:

: 100-39-0
benzyl bromide

: 89215-49-6,93170-22-0,93170-23-1
(2R,3ξ)-1,2-O-isopropylidene-4-<2-(5-methylfuryl)>-1,2,3-butanetriol

: 93170-25-3
(2R,3R)-3-O-benzyl-1,2-O-isopropylidene-4-<2-(5-methylfuryl)>-1,2,3-butanetriol

: 93170-24-2
(2R,3S)-3-O-benzyl-1,2-O-isopropylidene-4-<2-(5-methylfuryl)>-1,2,3-butanetriol

Guidance literature:: With sodium hydride; Yield given. Multistep reaction. Yields of byproduct given; 1.) THHF, DMF, rt., 0.5 h, 2.) THF, DMF, 12 h;
DOI:10.1016/S0040-4020(01)86159-7