anti-octahydronaphthalene-2,3,6,7-tetracarboximide

Base Information

• Chemical Name: anti-octahydronaphthalene-2,3,6,7-tetracarboximide
• CAS No.: 103617-35-2
• Molecular Formula: C₃₈H₃₀N₂O₄
• Molecular Weight: 578.667
• Mol file: 103617-35-2.mol

Synonyms:anti-octahydronaphthalene-2,3,6,7-tetracarboximide

Chemical Property of anti-octahydronaphthalene-2,3,6,7-tetracarboximide

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of anti-octahydronaphthalene-2,3,6,7-tetracarboximide

There total 3 articles about anti-octahydronaphthalene-2,3,6,7-tetracarboximide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 74.0%

N-phenyl-maleimide (941-69-5) + (E,E)-1,2-dibenzylidenecyclobutane (94618-65-2) → anti-octahydronaphthalene-2,3,6,7-tetracarboximide (103617-35-2)

Guidance literature:

In toluene; at 150 ℃; for 30h;

DOI:10.1021/jo00369a003 DOI:10.1039/c39840001046

Reference yield:

benzaldehyde (100-52-7) → anti-octahydronaphthalene-2,3,6,7-tetracarboximide (103617-35-2)

Guidance literature:

Multi-step reaction with 2 steps

1: 70 percent / (EtO)2P(O)Li / tetrahydrofuran; dimethylformamide / 24 h / Ambient temperature

2: 74 percent / toluene / 30 h / 150 °C

With diethyl phosphite lithium salt; In tetrahydrofuran; N,N-dimethyl-formamide; toluene;

DOI:10.1039/c39840001046

Reference yield:

benzaldehyde (100-52-7) → anti-octahydronaphthalene-2,3,6,7-tetracarboximide (103617-35-2)

Guidance literature:

Multi-step reaction with 2 steps

1: 70 percent / tetrahydrofuran; dimethylformamide / 24 h / Ambient temperature

2: 74 percent / toluene / 30 h / 150 °C

In tetrahydrofuran; N,N-dimethyl-formamide; toluene;

DOI:10.1021/jo00369a003

upstream raw materials:

N-phenyl-maleimide

(E,E)-1,2-dibenzylidenecyclobutane

benzaldehyde