1-(hexyl-6'-bromo)-2,5-dimethoxybenzene

Base Information

• Chemical Name: 1-(hexyl-6'-bromo)-2,5-dimethoxybenzene
• CAS No.: 151426-30-1
• Molecular Formula: C₁₄H₂₁BrO₂
• Molecular Weight: 301.224
• Mol file: 151426-30-1.mol

Synonyms:1-(hexyl-6'-bromo)-2,5-dimethoxybenzene

Chemical Property of 1-(hexyl-6'-bromo)-2,5-dimethoxybenzene

Chemical Property:

Purity/Quality:

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MSDS Files:

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Technology Process of 1-(hexyl-6'-bromo)-2,5-dimethoxybenzene

There total 1 articles about 1-(hexyl-6'-bromo)-2,5-dimethoxybenzene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

1 ,6-dibromohexane (629-03-8) + 1,4-dimethoxybezene (150-78-7) → 1-(hexyl-6'-bromo)-2,5-dimethoxybenzene (151426-30-1)

Guidance literature:

With n-butyllithium; Yield given. Multistep reaction; 1.) THF, 0 deg C, 1 h, 2.) THF, RT, 1 h;

DOI:10.1021/ja00078a012

Reference yield: 92.0%

1-(hexyl-6'-bromo)-2,5-dimethoxybenzene (151426-30-1) + N-methylaniline (100-61-8) → [6-(2,5-Dimethoxy-phenyl)-hexyl]-methyl-phenyl-amine (151426-31-2)

Guidance literature:

With tetrabutylammomium bromide; potassium carbonate; sodium iodide; In toluene; for 5h; Heating;

DOI:10.1021/ja00078a012

Reference yield: 80.0%

1-(hexyl-6'-bromo)-2,5-dimethoxybenzene (151426-30-1) → 1-iodo-4-hexyl-6'-bromo-2,5-dimethoxybenzene

Guidance literature:

With potassium iodate; iodine; In sulfuric acid; acetic acid; for 4h; Heating;

DOI:10.1021/j100014a003

upstream raw materials:

1 ,6-dibromohexane

1,4-dimethoxybezene

Downstream raw materials:

[6-(2,5-Dimethoxy-phenyl)-hexyl]-methyl-phenyl-amine

2-(6-carbazol-9-ylhexyl)-1,4-dimethoxybenzene

2-(6-carbazol-9-ylhexyl)-1,4-hydroquinone

4-{[6-(2,5-Dimethoxy-phenyl)-hexyl]-methyl-amino}-benzaldehyde