[bis(trimethylsilyl)methyl](2,4,6-tris[bis(trimethylsilyl)methyl]phenyl)stannane

Base Information

Chemical Name:[bis(trimethylsilyl)methyl](2,4,6-tris[bis(trimethylsilyl)methyl]phenyl)stannane
CAS No.:820217-38-7
Molecular Formula:C₃₄H₈₀Si₈Sn
Molecular Weight:832.403
Hs Code.:

Synonyms:[bis(trimethylsilyl)methyl](2,4,6-tris[bis(trimethylsilyl)methyl]phenyl)stannane

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of [bis(trimethylsilyl)methyl](2,4,6-tris[bis(trimethylsilyl)methyl]phenyl)stannane

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Technology Process of [bis(trimethylsilyl)methyl](2,4,6-tris[bis(trimethylsilyl)methyl]phenyl)stannane

There total 3 articles about [bis(trimethylsilyl)methyl](2,4,6-tris[bis(trimethylsilyl)methyl]phenyl)stannane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 59.0%

: 820217-36-5
dichloro[bis(trimethylsilyl)methyl](2,4,6-tris[bis(trimethylsilyl)methyl]phenyl)stannane

: 820217-38-7
[bis(trimethylsilyl)methyl](2,4,6-tris[bis(trimethylsilyl)methyl]phenyl)stannane

Guidance literature:: With LiAlH₄; In tetrahydrofuran; (Ar); Sn compd. added to a suspn. of LiAlH4, stirred for 13 h, treated with addnl. LiAlH4, refluxed for 1 h; cooled to room temp., treated with EtOAc and H2O, evapd., subjected to dry-column chromy.;
DOI:10.1021/ja048453h

Reference yield:

: 115160-05-9
1-bromo-2,4,6-tris[bis(trimethylsilyl)methyl]benzene

: 820217-38-7
[bis(trimethylsilyl)methyl](2,4,6-tris[bis(trimethylsilyl)methyl]phenyl)stannane

Guidance literature:: Multi-step reaction with 2 steps

1: t-BuLi; Mg / pentane; tetrahydrofuran

2: LiAlH₄ / tetrahydrofuran

With t-BuLi; Mg; LiAlH₄; In tetrahydrofuran; pentane;
DOI:10.1021/ja048453h

Reference yield:

: 5926-35-2
chlorobis(trimethylsilyl)methane

: 820217-38-7
[bis(trimethylsilyl)methyl](2,4,6-tris[bis(trimethylsilyl)methyl]phenyl)stannane

Guidance literature:: Multi-step reaction with 2 steps

1: t-BuLi; Mg / pentane; tetrahydrofuran

2: LiAlH₄ / tetrahydrofuran

With t-BuLi; Mg; LiAlH₄; In tetrahydrofuran; pentane;
DOI:10.1021/ja048453h