(9S,11R,15R)-11,15-bis(tetrahydropyran-2-yloxy)-15-cyclohexyl-2,3,4,5,6,16,17,18,19,20-decanor-9-(triethylsiloxy)prostanal

Base Information

Chemical Name:(9S,11R,15R)-11,15-bis(tetrahydropyran-2-yloxy)-15-cyclohexyl-2,3,4,5,6,16,17,18,19,20-decanor-9-(triethylsiloxy)prostanal
CAS No.:170290-73-0
Molecular Formula:C₃₂H₅₈O₆Si
Molecular Weight:566.894
Hs Code.:

Synonyms:(9S,11R,15R)-11,15-bis(tetrahydropyran-2-yloxy)-15-cyclohexyl-2,3,4,5,6,16,17,18,19,20-decanor-9-(triethylsiloxy)prostanal

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Chemical Property of (9S,11R,15R)-11,15-bis(tetrahydropyran-2-yloxy)-15-cyclohexyl-2,3,4,5,6,16,17,18,19,20-decanor-9-(triethylsiloxy)prostanal

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Technology Process of (9S,11R,15R)-11,15-bis(tetrahydropyran-2-yloxy)-15-cyclohexyl-2,3,4,5,6,16,17,18,19,20-decanor-9-(triethylsiloxy)prostanal

There total 1 articles about (9S,11R,15R)-11,15-bis(tetrahydropyran-2-yloxy)-15-cyclohexyl-2,3,4,5,6,16,17,18,19,20-decanor-9-(triethylsiloxy)prostanal which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 87.0%

: 170290-72-9
(9S,11R,15R)-11,15-bis(tetrahydropyran-2-yloxy)-15-cyclohexyl-2,3,4,5,6,16,17,18,19,20-decanor-9-(triethylsiloxy)prostanol triethyl silyl ether

: 170290-73-0
(9S,11R,15R)-11,15-bis(tetrahydropyran-2-yloxy)-15-cyclohexyl-2,3,4,5,6,16,17,18,19,20-decanor-9-(triethylsiloxy)prostanal

Guidance literature:: With oxalyl dichloride; dimethyl sulfoxide; triethylamine; In dichloromethane; at -60 - 5 ℃;
DOI:10.1016/S0968-0896(02)00016-0

Reference yield: 69.0%

: 88738-78-7
bis-(2,2,2-trifluoroethyl)(methoxycarbonylmethyl)phosphonate

: 170290-73-0
(9S,11R,15R)-11,15-bis(tetrahydropyran-2-yloxy)-15-cyclohexyl-2,3,4,5,6,16,17,18,19,20-decanor-9-(triethylsiloxy)prostanal

: 170290-74-1
(5Z)-(9S,11R,15R)-11,15-bis(tetrahydropyran-2-yloxy)-15-cyclohexyl-2,3,4,16,17,18,19,20-octanor-9-(triethylsiloxy)-5-prostenoic acid methyl ester

: (5E)-(9S,11R,15R)-11,15-bis(tetrahydropyran-2-yloxy)-15-cyclohexyl-2,3,4,16,17,18,19,20-octanor-9-(triethylsiloxy)-5-prostenoic acid methyl ester

Guidance literature:: bis-(2,2,2-trifluoroethyl)(methoxycarbonylmethyl)phosphonate; With Tris(3,6-dioxaheptyl)amine; potassium hexamethylsilazane; In tetrahydrofuran; toluene; at -65 ℃; for 1h;

(9S,11R,15R)-11,15-bis(tetrahydropyran-2-yloxy)-15-cyclohexyl-2,3,4,5,6,16,17,18,19,20-decanor-9-(triethylsiloxy)prostanal; In tetrahydrofuran; toluene; at -50 - -20 ℃;
DOI:10.1016/S0968-0896(02)00016-0