(5Z)-(9S,11R,15R)-11,15-bis(tetrahydropyran-2-yloxy)-15-cyclohexyl-2,3,4,16,17,18,19,20-octanor-9-(triethylsiloxy)-5-prostenoic acid methyl ester

Base Information

Chemical Name:(5Z)-(9S,11R,15R)-11,15-bis(tetrahydropyran-2-yloxy)-15-cyclohexyl-2,3,4,16,17,18,19,20-octanor-9-(triethylsiloxy)-5-prostenoic acid methyl ester
CAS No.:170290-74-1
Molecular Formula:C₃₅H₆₂O₇Si
Molecular Weight:622.959
Hs Code.:

Synonyms:(5Z)-(9S,11R,15R)-11,15-bis(tetrahydropyran-2-yloxy)-15-cyclohexyl-2,3,4,16,17,18,19,20-octanor-9-(triethylsiloxy)-5-prostenoic acid methyl ester

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Chemical Property of (5Z)-(9S,11R,15R)-11,15-bis(tetrahydropyran-2-yloxy)-15-cyclohexyl-2,3,4,16,17,18,19,20-octanor-9-(triethylsiloxy)-5-prostenoic acid methyl ester

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Technology Process of (5Z)-(9S,11R,15R)-11,15-bis(tetrahydropyran-2-yloxy)-15-cyclohexyl-2,3,4,16,17,18,19,20-octanor-9-(triethylsiloxy)-5-prostenoic acid methyl ester

There total 1 articles about (5Z)-(9S,11R,15R)-11,15-bis(tetrahydropyran-2-yloxy)-15-cyclohexyl-2,3,4,16,17,18,19,20-octanor-9-(triethylsiloxy)-5-prostenoic acid methyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 69.0%

: 88738-78-7
bis-(2,2,2-trifluoroethyl)(methoxycarbonylmethyl)phosphonate

: 170290-73-0
(9S,11R,15R)-11,15-bis(tetrahydropyran-2-yloxy)-15-cyclohexyl-2,3,4,5,6,16,17,18,19,20-decanor-9-(triethylsiloxy)prostanal

: 170290-74-1
(5Z)-(9S,11R,15R)-11,15-bis(tetrahydropyran-2-yloxy)-15-cyclohexyl-2,3,4,16,17,18,19,20-octanor-9-(triethylsiloxy)-5-prostenoic acid methyl ester

: (5E)-(9S,11R,15R)-11,15-bis(tetrahydropyran-2-yloxy)-15-cyclohexyl-2,3,4,16,17,18,19,20-octanor-9-(triethylsiloxy)-5-prostenoic acid methyl ester

Guidance literature:: bis-(2,2,2-trifluoroethyl)(methoxycarbonylmethyl)phosphonate; With Tris(3,6-dioxaheptyl)amine; potassium hexamethylsilazane; In tetrahydrofuran; toluene; at -65 ℃; for 1h;

(9S,11R,15R)-11,15-bis(tetrahydropyran-2-yloxy)-15-cyclohexyl-2,3,4,5,6,16,17,18,19,20-decanor-9-(triethylsiloxy)prostanal; In tetrahydrofuran; toluene; at -50 - -20 ℃;
DOI:10.1016/S0968-0896(02)00016-0