N-[5-(Diethylamino)-2-[(2,4-dinitrophenyl)azo]phenyl]acetamide

Base Information

• Chemical Name: N-[5-(Diethylamino)-2-[(2,4-dinitrophenyl)azo]phenyl]acetamide
• CAS No.: 24112-48-9
• Molecular Formula: C18H20 N6 O5
• Molecular Weight: 400.394
• Hs Code.: 2927000090
• European Community (EC) Number: 246-022-6
• DSSTox Substance ID: DTXSID401040803
• Nikkaji Number: J242.734F
• Mol file: 24112-48-9.mol

Synonyms:24112-48-9;EINECS 246-022-6;N-[5-(DIETHYLAMINO)-2-[(2,4-DINITROPHENYL)AZO]PHENYL]ACETAMIDE;N-(5-(Diethylamino)-2-((2,4-dinitrophenyl)azo)phenyl)acetamide;N-5-(Diethylamino)-2-(2,4-dinitrophenyl)azophenylacetamide;SCHEMBL11418250;WCUXAQAVBINHFZ-UHFFFAOYSA-N;C18H20N6O5;DTXSID401040803;C18-H20-N6-O5;W-110584;3-acetylamino-4-(2',4'-dinitrophenylazo)-N,N-diethylaniline;N-[5-(Diethylamino)-2-(2,4-dinitrophenylazo)phenyl]acetamide;Acetamide, N-[5-(diethylamino)-2-[(2,4-dinitrophenyl)azo]phenyl]-;Acetamide, N-[5-(diethylamino)-2-[2-(2,4-dinitrophenyl)diazenyl]phenyl]-

Chemical Property of N-[5-(Diethylamino)-2-[(2,4-dinitrophenyl)azo]phenyl]acetamide

Chemical Property:

• Vapor Pressure: 9.44E-18mmHg at 25°C
• Boiling Point: 668.8°Cat760mmHg
• Flash Point: 358.3°C
• PSA: 152.19000
• Density: 1.35g/cm³
• LogP: 6.41890
• XLogP3: 3.4
• Hydrogen Bond Donor Count: 1
• Hydrogen Bond Acceptor Count: 8
• Rotatable Bond Count: 6
• Exact Mass: 400.14951776
• Heavy Atom Count: 29
• Complexity: 615

Purity/Quality:

99% ^*data from raw suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

• Canonical SMILES: CCN(CC)C1=CC(=C(C=C1)N=NC2=C(C=C(C=C2)[N+](=O)[O-])[N+](=O)[O-])NC(=O)C

Technology Process of N-[5-(Diethylamino)-2-[(2,4-dinitrophenyl)azo]phenyl]acetamide

There total 15 articles about N-[5-(Diethylamino)-2-[(2,4-dinitrophenyl)azo]phenyl]acetamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 98.8%

3-acetylamino-4-(2'-bromo-4',6'-dinitrophenylazo)-N,N-diethylaniline (52697-38-8) → 2'-acetamido-4'-diethylamino-2,4-dinitroazobenzene (24112-48-9) + 3-acetylamino-4-(2'-cyano-4',6'-dinitrophenylazo)-N,N-diethylaniline (24170-60-3)

Guidance literature:

With ; In acetonitrile; at 19.9 ℃; for 3.31667h; Rate constant; Mechanism; Product distribution; further reaction time;

Reference yield: 92.0%

3-acetylamino-4-(2'-bromo-4',6'-dinitrophenylazo)-N,N-diethylaniline (52697-38-8) → 2'-acetamido-4'-diethylamino-2,4-dinitroazobenzene (24112-48-9) + 2-acetamido-4-diethylamino-6-diethylphosphonato-2',4'-dinitroazobenzene (65000-79-5) + N-{2-[2'-(2-Acetylamino-4-diethylamino-phenylazo)-3,5,3',5'-tetranitro-biphenyl-2-ylazo]-5-diethylamino-phenyl}-acetamide (72974-40-4)

Guidance literature:

With (bpy)>; In ethanol; for 24h; Product distribution; Rate constant; Kinetics; different substituents in ArX, solvents, temperatures and light; other copper complexes; rate constants under other temperatures; activation energy;

Reference yield: 83.5%

m-acetylamino-N,N-diethylanilne (6375-46-8) + 2,4-Dinitroanilin (97-02-9) → N,N-diethyl-4-(2,4-dinitrophenylazo)-3-acetamidoaniline (24112-48-9)

Guidance literature:

2,4-Dinitroanilin; With tert.-butylnitrite; naphthalene-1,5-disulfonate; In diethylene glycol dimethyl ether; at 20 ℃; for 1h;

m-acetylamino-N,N-diethylanilne; With sodium carbonate; naphthalene-1,5-disulfonate; In water; at 0 ℃; for 0.166667h; pH=4 - 6; Solvent; Reagent/catalyst;

upstream raw materials:

m-acetylamino-N,N-diethylanilne

2,4-Dinitroanilin

3-acetylamino-4-(2'-bromo-4',6'-dinitrophenylazo)-N,N-diethylaniline

N-[5-Diethylamino-2-(2-iodo-4,6-dinitro-phenylazo)-phenyl]-acetamide