C₃₈H₃₄O₆

Base Information

• Chemical Name: C₃₈H₃₄O₆
• CAS No.: 1382734-78-2
• Molecular Formula: C₃₈H₃₄O₆
• Molecular Weight: 586.684
• Mol file: 1382734-78-2.mol

Synonyms:C₃₈H₃₄O₆

Chemical Property of C₃₈H₃₄O₆

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of C₃₈H₃₄O₆

There total 8 articles about C₃₈H₃₄O₆ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 96.0%

2,5-dibromo-p-xylene (1074-24-4) + methyl 2-(benzyloxy)-4-(pinacolboronic ester) benzoate (1073355-16-4) → C38H34O6 (1382734-78-2)

Guidance literature:

With (1,1'-bis(diphenylphosphino)ferrocene)palladium(II) dichloride; cesium fluoride; In 1,4-dioxane; water; Inert atmosphere; Reflux;

DOI:10.1002/chem.201201985

Reference yield: 96.0%

→ C38H34O6 (1382734-78-2)

Guidance literature:

With (1,1'-bis(diphenylphosphino)ferrocene)palladium(II) dichloride; cesium fluoride; In 1,4-dioxane; water; at 90 ℃; for 24h; Inert atmosphere;

Reference yield:

benzyl bromide (100-39-0) → C38H34O6 (1382734-78-2)

Guidance literature:

Multi-step reaction with 3 steps

1: potassium carbonate / acetonitrile / 80 °C / Inert atmosphere

2: potassium acetate; bis-triphenylphosphine-palladium(II) chloride / 1,4-dioxane / 16 h / Inert atmosphere; Reflux

3: cesium fluoride; (1,1'-bis(diphenylphosphino)ferrocene)palladium(II) dichloride / 1,4-dioxane; water / Inert atmosphere; Reflux

With bis-triphenylphosphine-palladium(II) chloride; (1,1'-bis(diphenylphosphino)ferrocene)palladium(II) dichloride; potassium acetate; potassium carbonate; cesium fluoride; In 1,4-dioxane; water; acetonitrile; 3: |Suzuki-Miyaura Coupling;

DOI:10.1002/chem.201201985

upstream raw materials:

methyl 4-iodosalicylate

2,5-dibromo-p-xylene

methyl 2-(benzyloxy)-4-(pinacolboronic ester) benzoate

benzyl bromide

Downstream raw materials:

3-mer-HCA