nonyl-diphenyl-stibine

Base Information

• Chemical Name: nonyl-diphenyl-stibine
• CAS No.: 70367-19-0
• Molecular Formula: C₂₁H₂₉Sb
• Molecular Weight: 403.211
• Mol file: 70367-19-0.mol

Synonyms:nonyl-diphenyl-stibine

Chemical Property of nonyl-diphenyl-stibine

Chemical Property:

Purity/Quality:

Safty Information:

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MSDS Files:

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Technology Process of nonyl-diphenyl-stibine

There total 11 articles about nonyl-diphenyl-stibine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 65.0%

nonylmagnesium bromide (39691-62-8) + diphenylantimony(III) chloride (2629-47-2) → nonyl-diphenyl-stibine (70367-19-0)

Guidance literature:

In diethyl ether;

Reference yield: 61.0%

1-Iodooctane (629-27-6) + {(diphenylstibino)methyl}copper(I) (70367-15-6) → nonyl-diphenyl-stibine (70367-19-0)

Guidance literature:

With potassium cyanide; In tetrahydrofuran; byproducts: CuI; soln. warmed from -20°C to room temp., stirred for 12 h, hydrolysis; shaken with ether, dried above Na2SO4, solvent evapd.;

Reference yield:

phenyllithium (591-51-5) → nonyl-diphenyl-stibine (70367-19-0)

Guidance literature:

Multi-step reaction with 3 steps

1: tetrahydrofuran

2: CuCl / tetrahydrofuran

3: tetrahydrofuran

With CuCl; In tetrahydrofuran;

upstream raw materials:

nonylmagnesium bromide

diphenylantimony(III) chloride

1-Iodooctane

{(diphenylstibino)methyl}copper(I)

Downstream raw materials:

nonyl-diphenyl antimony ⁽²⁺⁾; dibromide